Some standard content:
QB1643-1998
This standard is revised and compiled based on QB1643-1992 "Hair Mousse" and in accordance with GB/T1.1-1993 Standardization Work Guide Unit 1: Drafting and Expression Rules of Standards Part 1: Basic Regulations for Standard Compilation. As a mandatory industry standard, this standard deletes the residue and total solid index part in QB1643-1992 in its technical indicators: revised the appearance and pH value, added the spray rate and packaging mark: the test method adopts GB/T11419-1993 "Test Methods for Aerosol Products"; and its net content index is implemented in accordance with the quantitative packaging commodity measurement supervision regulations. This standard is proposed by the Industry Management Department of the State Light Industry Bureau. This standard is under the jurisdiction of the National Cosmetics Standardization Center. The drafting units of this standard are: Shanghai Jahwa Co., Ltd., Shanghai Daily Chemical Industry Research Institute. The main drafters of this standard are: Chen Yafang, Xue Zhigang, Du Baolin, Jiang Huimin. As of the date of implementation of this standard, the light industry standard QB1643-1992 "Hair Mousse" issued by the former Ministry of Light Industry shall be abolished. 1 Scope
Light Industry Standard of the People's Republic of China
Hair Mousse
QB1643-1998
Replaces QB1643-1992
This standard specifies the product classification, technical requirements, test methods, inspection rules and marking, packaging, transportation, storage and other requirements for hair mousse.
This standard applies to mousse made of propane or mixed gas containing dimethyl ether as propellant and high molecular polymer as raw material for fixing hair style or protecting, modifying and beautifying hair style. 2 Referenced Standards
The provisions contained in the following standards constitute the provisions of this standard through reference in this standard. When this standard is published, the versions shown are valid. All standards will be revised, and parties using this standard should explore the possibility of using the latest version of the following standards. GB5296.3-1995 Instructions for use of consumer products General labeling of cosmetics GB7916-1987 Hygienic standards for cosmetics GB/T7917.1-1987 Standard test methods for cosmetic hygiene and chemistry - Mercury GB/T7917.2-1987 Standard test methods for cosmetic hygiene and chemistry - Monument GB/T7917.3-1987 Standard test methods for cosmetic hygiene and chemistry - Lead GB/T13531.1-1992 General test methods for cosmetics - Determination of pH value GB/T14449-1993 Test methods for aerosol products BB0005-1995 Labeling of Aerosol Products
QB/T1684—1993 Inspection Rules for Cosmetics QB/T1685—1993 Requirements for the Appearance of Cosmetics Packages State Bureau of Technical Supervision Order (95) No. 43 Regulations on Metrological Supervision of Quantitatively Packaged Goods 3 Terminology
Hair mousse
A foam aerosol product used for hair styling, care and hair modification and beautification. 4 Product Classification
According to the function of hair mousse, it is divided into styling mousse, hair care mousse and hair modification and beautification mousse. 5 Technical Requirements
The raw materials used for hair mousse shall comply with the requirements of GB7916. 5.1 Sensory, physical and chemical and hygiene indicators shall be as specified in Table 1. Sensory index
Physical and chemical index
Hygiene index
5.2 Net content
Heat resistance
Block resistance
Ejection rate, 9
Leakage test
Internal pressure, MPa
Mercury, mg/kg
Lead (in Pb), mg/kg
Arsenic (in As), mg/kg
Methanol, %
QB1643-1998
The foam is uniform. The texture is delicate and highly elastic
The specified fragrance
40℃4h, normal use after recovery to air temperature 0℃~-5℃24h. Normal use after recovery to room temperature≥95
No leakage in the 50℃ constant temperature water bath. The test in the 25℃ constant temperature water bath should be less than 0.840
The net content of a single piece of quantitatively packaged product should comply with the table (I) of the State Technical Supervision Bureau Order (95) No. 43: The average deviation of batch quantitatively packaged products 4Q≥0.
5.3 Packaging appearance requirements
Should comply with the provisions of 3.6, 3.10.2, and 3.10.3 of QB/T1685-1993. 6 Test method
6.1 Appearance
Spray the sample according to the product usage method, visually inspect, and touch it with your fingers. The foam is uniform, delicate and elastic. 6.2 Aroma
Spray on the scent paper according to the product usage instructions, intermittently, and identify whether the aroma meets the specified aroma type. 6.3 pH
6.3.1 Instrument
A balance: accuracy 0.1g;
A pH meter: accuracy ± 0.02.
6.3.2 Sample preparation
Take a sample and weigh its mass W, (g) on the balance. According to the usage instructions, put about 1g of the sample into a 250mL beaker, and then weigh the mass of the sample after the sample is released, W, (g). Use the measurement method to calculate the sample volume: W=W,-W.6.3.3 Determination method
Determine according to GB/T13531.1.
6.4 Heat resistance
Pre-adjust the constant temperature water bath to (40±2)℃, put a bottle of the sample with complete packaging into the constant temperature water bath, keep it warm for 4 hours, take it out, restore it to room temperature, and observe it according to the normal use method. 6.5 Cold resistance
Pre-adjust the refrigerator to 0℃～5℃, put a bottle of the sample with complete packaging into the refrigerator, leave it for 24 hours, take it out, restore it to room temperature, and observe it according to the normal use method.
6.6 Spray rate
Measure according to 4.10 of GB/T14449-1993. 6.7 Leakage test
QB1643-1998
Pre-adjust the constant temperature water bath to (50工2)℃, then put two bottles of samples in and shake them well, put the sample with the plastic cover removed upright into the water bath, and no more than 5 bubbles appear in each can of bone within 5 minutes to be qualified. 6.8 Internal pressure
Measured according to 4.1 of GB/T14449-1993. 6.9 Mercury
Measured according to GB/T7917.1
Measured according to GB/T7917.2.
Measured according to GB/T7917.3.
6.12 Methanol
6.12.1 Reagents
6.12.1.1 Methanol-free ethanol, take 1.0μL of anhydrous ethanol (superior grade) and inject it into the chromatograph, and no impurity peaks should appear. 6.12.1.2 Ethanol (CH0H=75%): Take 75mL of ethanol (6.12.1.1) and dilute it to 100mL with pure water. 6.12.1.3 Gas chromatograph reagent: GDX-102 (60-~80 mesh). 6.12.1.4 Gas chromatography reagents: polyethylene glycol 1540 (or 1500). Methanol standard solution (CH, OH = 1%), take 1.0 mL of chromatographic-grade methanol and place it in a 100 mL volumetric flask, and dilute to the mark with 75% ethanol 6.12.1.5
(6.12.1.2). Store in a refrigerator. 6.12.1.6 Sodium chloride: analytical grade.
6.12.1.7 Defoaming agent: emulsified silicone oil, such as 284PS, from Shanghai Resin Factory. 6.12.2 Instruments
6.12.2.1 Gas chromatograph: with hydrogen flame ionization detector. 6.12.2.2wwW.bzxz.Net
Chromatographic column: 2 m × 2 mm, filled with GDX-102. Applicable to samples that do not contain dimethyl ether. Chromatographic column: Specifications: 2m×4mm, filled with GDX-102 (6.12.1.3) 6.12.2.31
carrier coated with 25% polyethylene glycol 1540 (or 1500). This chromatographic column is suitable for samples containing diformaldehyde. 6.12.2.4 All-glass ground mouth water-steaming device. 6.12.2.5
Super constant temperature water bath: temperature range 0℃~100℃, temperature control accuracy ±0.5℃. 6.12.2.6 Syringe: 0.5mL.1L, 1mL. 6.12.3 Analysis steps
6.12.3.1 Start the chromatograph
Make necessary adjustments to achieve the best working conditions of the instrument. The chromatographic conditions are selected according to the specific situation. The reference conditions are: A) Chromatographic conditions 1 (applicable to samples without diformaldehyde) Column temperature: 170C; Vaporization chamber and detector temperature: 200℃; Nitrogen flow rate: 40mL/min: Hydrogen flow rate: 40ml./min, air flow rate: 500mL/min (the flow rate can be adjusted according to the specific instrument).
b) Chromatographic conditions 2 (applicable to samples containing dimethyl ether) Column temperature: 75C, vaporization temperature 90℃: detector temperature: 150℃; nitrogen flow rate: 30mL/min; hydrogen flow rate: 30mL/min air flow rate: 300mL/min (the flow rate can be adjusted according to the specific instrument).
QB1643-1998
Put a certain amount of 75% ethanol (6.12.1.2) in a hot filling bottle, replace the original nozzle with a nozzle with a catheter, insert the other end of the catheter below the ethanol liquid surface, and slowly press the nozzle to make the sample flow into the ethanol solution. Calculate the sampling volume using the difference subtraction method. 6.12.3.3 Sample pretreatment (stuffing method)
Take 10mL of sample and add 50mL of steaming water, 2g of sodium chloride (6.12.1.6), 1 drop of defoamer (6.12.1.7) and 30mL of methanol-free ethanol (6.12.1.1) to a steaming bottle. Steam the stuffing in a boiling water bath, collect about 40mL of distillate in a 50mL volumetric flask, add methanol-free ethanol to the mark, and use this as the sample solution.
6.12.3.4 Drawing of standard curve
Take 7 50mL volumetric flasks, add methanol standard solution (6.12.1.5): 0.25, 0.50, 1.00, 2.00, 4.00, 7.0010.00mL respectively, and then add 75% ethanol (6.12.1.2) to the mark respectively. The methanol content of this standard series is: 0.005%, 0.01%, 0.02%, 0.04%, 0.08%, 0.14%, 0.20%.
6.12.3.5 Determination
Take 1uL of the sample solution to be tested and 1L of the standard solution in turn, inject into the gas chromatograph, record the peak area of each chromatogram and draw the peak area-methanol concentration (V/V) curve.
6.12.4 Calculation
Where: 一一the volume fraction of methanol in the sample, %; P - the volume fraction of methanol in the sample solution obtained from the standard curve, %, K - the sample dilution factor.
6.13 Net content
Determined in accordance with the Order of the State Technical Supervision Bureau (95 No. 43. 7 Inspection rules
According to QB/T1684.
8 Marking, packaging, transportation, storage
8.1 Sales packaging marking
According to the requirements of GB5296.3 and BB0005. 8.2 Transport packaging marking
Should include product name, trademark, manufacturer's name and address, standard number, net content, quantity, gross weight, volume, storage and transportation diagram, production period and shelf life, or production batch number and final use date.
8.3 Packaging
Bottles can be packed in corrugated paper according to the needs of the manufacturer, and there are corrugated paper clips in the middle packaging paper. Double corrugated paper boxes are used for large packages, and there is no space inside. The qualified mark or certificate is placed. 8.4 Transportation
Must be placed and unloaded gently, and stacked according to the arrow mark on the box to avoid severe vibration, impact, sun and rain. 8.5 Storage
8.5.1 It should be stored in a ventilated and dry warehouse with a temperature not higher than 38C, and should not be close to the stove heater. When stacking, it must be 20cm from the ground and 50cm from the wall. There should be a passage in the middle. Stack according to the arrow on the box and do not put it upside down. If it is a dangerous product, it should be stored in accordance with the requirements for dangerous goods. 8.5.2 Shelf life
Under the specified transportation and storage conditions, the shelf life of the product shall be implemented in accordance with the relevant shelf life regulations in QB/T1685 when the packaging is intact and unsealed.
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