Some standard content:
Chemical Industry Standard of the People's Republic of China
HG2283—92
Reaction Black KN-8BG
(Active Black KN-B)
Published on June 1, 1992
Ministry of Chemical Industry of the People's Republic of China
Implemented on January 1, 1993
W Chemical Industry Standard of the People's Republic of China
Reaction Black KN-8BG
(Active Black KN-B)
Subject Content and Scope of Application
HG2283—92
This standard specifies the technical requirements, test methods, inspection rules and marking, packaging, transportation and storage requirements of reaction black KN-8BG.
This standard applies to reaction black KN-8BG prepared by using p-β-vinyl sulfate aniline as raw material, after diazotization, and then coupling with H acid twice.
Structural formula:Www.bzxZ.net
NaO.socH.O,S
Molecular formula: C26H21O19NSeNa4
Relative molecular mass: 991.83 (according to the international relative atomic mass in 1989) 2 Reference standards
GB2374
GB2381
GB2383
GB2386
GB2387
GB2390
GB2391
GB2392
GB3920
GB3921
GB3922
GB6152
GB8427
G B8433
General conditions for dyeing determination
Determination method of insoluble matter content in dyes
Determination method of screening fineness of dyes
Determination method of moisture content in dyes and dye intermediatesDetermination method of color shade and intensity of reactive dyesDetermination method of pH value of reactive dyes
Determination method of color absorption and fixation rate of reactive dyesDetermination method of thermal stability of disperse dyes
Test method for color fastness of textiles to rubbing
Test method for color fastness of textiles to washing
Test method for color fastness of textiles to perspiration
Test method for color fastness of textiles to hot pressing (ironing)Test method for color fastness of textiles to lightTest method for color fastness of textiles to chlorinated swimming pool water by xenon arc test methodHG 2—801
Determination of solubility of reactive dyes
3 Technical requirements
3.1 Appearance: black uniform powder.
3.2 The quality of reaction black KN-8BG shall conform to the requirements of Table 1. Approved by the Ministry of Chemical Industry of the People's Republic of China on June 1, 1992 SO2C2H.oSO3Na
Implementation on January 1, 1993
W.bzsoso, cOn(1) Strength, points
(2) Color light
(3) Content of impurities insoluble in water, %
(4) Moisture, %
(5) Fineness P (content of residue passing 250um sieve), %(6) Solubility (50℃), g/L
(7) pH value
(8) Color fixation rate, %
(9) Thermal stability
HG2283-92
Note: 1) The fineness index of low dust dosage forms and granular dosage forms is exempt from inspection. Refers to the standard product of 100
similar to the standard product~slightly
the color light is basically unchanged, and the intensity decreases ≤5%9
3.3 The color fastness of the reaction black KN-8BG sample on cotton fabric shall not be lower than the requirements of Table 2. Table 2
(Chlorine arc)
Washing resistance (95℃)
Perspiration (acid)
Note: 1/1 standard depth is equivalent to 3%owf. 4
Test method
4.1 Appearance
Measured by visual method.
Dyeing strength and color light
4~54~5
Perspiration (alkali)
4~53~4
(200℃, 4h later)
According to the provisions of GB2387. The dyeing depth is 2%, the anhydrous sodium sulfate is 50g/L, the trisodium phosphate is 6g/L, the color absorption temperature is 60℃, and the color fixing temperature is 60℃. The formula is shown in Table 3Table 3
Dye bath components
2g/500mL standard solution
2g/500mL sample solution
10% (m/m) anhydrous sodium sulfate solution
10% (m/m) trisodium phosphate solution l)
Add distilled water to
Note: 1) Trisodium phosphate is added during color fixing. Number
Number the cotton yarn (cloth) treated according to the regulations, boil it in clean water for 15 minutes, wash and wring it, then dye it in sequence at 60℃, stir it frequently within 15 minutes, and then stir it every 5 minutes, and dye it for 30 minutes in total. Then, lift the dyed sample from the liquid surface, add the required trisodium phosphate to fix the color, the fixing temperature is still 60℃, the time is 45 minutes, stir it frequently within the first 20 minutes, and then stir it every 5 minutes. After dyeing, wash it with clean water and wring it, and then perform soap washing.
4.3 Determination of water-insoluble impurities
W.bzsoso:com According to the relevant provisions in GB2381.
4.4 Determination of moisture
According to the provisions of "drying method" in GB2386. 4.5 Determination of fineness
According to the provisions of GB2383.
4.6 Determination of solubility
Perform according to the provisions of HG2-801.
4.7 Determination of pH value
Perform according to the provisions of GB2390.
4.8 Determination of color fixation
Perform according to the provisions of GB2391.
4.9 Determination of thermal stability
Perform according to the provisions of GB2392.
4.10 Determination of color fastness on cotton fabrics 4.10.1 Determination of color fastness to light
Perform according to the provisions of GB8427.
4.10.2 Determination of color fastness to washing
Perform according to the provisions of Method 4 in GB3921.
4.10.3 Determination of color fastness to rubbing
Perform according to the provisions of GB3920.
4.10.4 Determination of color fastness to perspiration
Perform in accordance with the provisions of GB3922.
4.10.5 Determination of color fastness to hot pressing
Perform in accordance with the provisions of GB6152.
4.10.6 Determination of color fastness to chlorinated swimming pool water shall be carried out in accordance with the provisions of GB8433.
5 Inspection rules
5.1 Inspection classification
HG2283—92
Items (1) and (7) in Chapter 3 are factory inspection items; items (8) and (9) are periodic inspection items, which shall be carried out once a month. All items in Chapter 3 are type inspection items. If one of the six situations specified in 6.6.1 of GB1.3 occurs, type inspection shall be carried out. In normal production, it shall be carried out once a year. 5.2 Sampling method
Random sampling is carried out in batches. For manufacturers, uniform products mixed once are considered a batch. For users, products with the same batch number from the same manufacturer are considered a batch. The number of samples shall not be less than √N
(N is the number of barrels of each batch of products). When sampling in small batches, the number of samples shall not be less than 3 barrels.
When sampling, do not allow foreign impurities to fall into the product. Use a stainless steel (or aluminum, copper) sampling tube to sample from the top, middle and bottom. After the sample is fully mixed and divided, take about 200g and divide it into two clean and dry ground-mouth bottles. Seal them with paraffin wax, attach labels, indicate the manufacturer name, product name, batch number, and sampling date, one bottle for inspection, and one bottle for future reference. 5.3 Manufacturer inspection
Reaction black KN-8BG should be inspected by the quality supervision department of the manufacturer. The manufacturer shall ensure that all reaction black KN-8BG shipped out of the factory meets the requirements of this standard and is accompanied by a quality certificate in a certain format. 3
Wbzsoso，cO5.4 User acceptance
HG2283—92
The user has the right to verify the reaction black KN-8BG received in accordance with the provisions of this standard. When the supply and demand parties have objections to the product quality, the two parties can negotiate to resolve the issue.
5.5 Re-inspection
If the inspection results do not meet the requirements of this standard, samples should be taken from twice the amount of packaging barrels for re-inspection. Even if only one indicator is unqualified in the re-inspection results, the entire batch of products cannot be regarded as qualified products. 5.6 Arbitration
When arbitration is required, the arbitration institution shall be determined by negotiation between the two parties. The arbitration method shall be in accordance with the provisions of this standard. 6 Marking, packaging, transportation, purchase and storage
6.1. The packaging barrel should have firm and clear markings, indicating the manufacturer's name, product name, registered trademark, factory batch number, date, standard number, specifications, gross weight and net weight, and the barrel should be accompanied by a product quality certificate. 6.2 Reaction black KN-8BG should be packaged in iron barrels lined with plastic bags, 35kg per barrel. Other packaging can be ordered according to user requirements. 6.3 Handle with care during transportation, prevent fire, sun and rain, and do not damage the packaging. 6.4 The product should be stored in a cool, dry and ventilated warehouse with a storage period of 1 year. Additional instructions:
This standard was proposed by the Science and Technology Department of the Ministry of Chemical Industry of the People's Republic of China. This standard is under the technical jurisdiction of the Shenyang Chemical Industry Research Institute of the Ministry of Chemical Industry. This standard was drafted by Tianjin Dye Factory. The main drafters of this standard are Wang Limin, Lin Xiuzhi and Lu Xiuqin. 4
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