This standard specifies the requirements, test methods, inspection rules and marking, packaging, transportation and storage of a-amyl cinnamaldehyde. This standard is applicable to the analysis and evaluation of the quality of a-amyl cinnamaldehyde obtained by chemical synthesis using heptanal and benzaldehyde as raw materials. QB/T 2614-2003 α-amyl cinnamaldehyde QB/T2614-2003 Standard download decompression password: www.bzxz.net

[CS 71 1CC. 60
Classification number: Y4°
Request number: 13158204
Light Industry Standard of the People's Republic of China
QB/T2614—2003
Replaces QB/T3762—1909
α-Amylcinnamaldehyde
-Amyl cinnamicaldehyde
2003-12-11 Issued
National Development and Reform Commission of the People's Republic of China 2004-05-01 Implementation
QE/T26142003
This standard is a revision of QB/3762-1999%-pentylphenylcarbaldehyde", and the content index should be combined into a variety of indicators, and the solubility indicator should be added.
The standard revision point is the US Food Chemical Codex PCCIV α-based fermentation. The standard is consistent with the US Food Chemical Codex V when the efficacy test method is withdrawn from the social filling: the test method can be used for most of the SO materials. The standard has been recorded in the information of the China Light Industry Federation. The original standard is the national fragrance and cosmetics environmental chemical technology Technical Committee. Shenzhen Haige Research Institute introduced the standard book "Shenzhen Huang Chemical Co., Ltd. The main drafters of this standard are: Xu Yi, Zhang Yangmen, Yuan Longquan. This standard was first issued in February 1988 as the national standard Gi3/8799-1988, and was converted into the industry standard QB3762-1999 in April 1999. The date of implementation of this standard is to replace the national light 1 The light industry standard QB/Jiangsu 371999 α-amyl cinnamaldehyde released by the industry this week is HKAONYKA
QB/T2614-2C03
1 specificationwww.bzxz.net
α-amyl cinnamaldehyde
, which does not define the requirements, test methods, inspection rules and specifications, packaging, transportation and storage of α-amyl cinnamaldehyde. This standard is used for: The quality of α-synthetic meat ferment is analyzed and negotiated. 2 Normative referenced documents
The following documents shall become the terms of this standard through the signed version and shall be applied to this standard. For all dated referenced documents, all final versions (excluding the validity period) or revised versions after the reference date shall apply to this standard. However, the parties that have reached an agreement based on this standard are encouraged to study whether the latest version of this document can be used: For undated documents, the latest version shall apply to this standard. Section B/Section 11540 Determination of the content of monostyrene and synthetic spices GB/14454.2 Evaluation method for aroma of raw materials
GB/T14454.3 Determination of color of raw materials
GB/T14454.4 Determination of refractive index of spices GB/T14454.12 Determination of trace chlorine in raw materials G13/T14454.17 Content of benzoic acid and benzoic acid compounds in spices Determination of the amount of alcohol by the drop-in-difference method GB/14453.1 Determination of the solubility of isolated and synthetic aromatic substances in ethanol by the solubility test method B44.4 Determination of the acid value of isolated and synthetic aromatic substances by the solubility test method 3 Product chemical name, molecular formula, structural formula, molecular weight Chemical name: 2-n-pentyl-3-propanedialdehyde Molecular formula: C
Structural formula:
(CH2)CH
Molecular weight: 202.28 (m 19 87 No. 4 Requirements
4.1 Color: yellow free liquid level
4.2 Odor: strong floral, jasmine-like fragrance.4.3 Refractive index (25C/25>): 0.9630.908.4.4 Refractive index (20): 1.5540~155904.5 Temperature (25℃): 1 mL of sample is dissolved in 5 mL of 80% (V/V)/ethanol: 4.6: 55.0.
4.7 Micro-reaction: reaction.
4.8Content (%: 9.0.
5Test methods
5.1Determination of color
See GB/T 14454.3.
5.2Assessment of aroma
J, GB/T 14454.2:
5.3Determination of relative density: 25℃/25℃GA/T11540
5.4Determination of refractive index, 20℃
GB/T14454.4
5.5Determination of solubility in ethanol, 25
.M GB/T 14457. 1:
5.6Determination of acid value
2 GH/T 14457.4
5.7 Determination of trace chlorine
See GB/T:1 14445.12
5.8 Determination of aldehyde content, measured as α-amyl carboxylic acid, see GB/T:4454.17:
Note: α-amyl carboxylic acid typical (color sheep diagram (area-based method) Shen A (qualification record) B inspection rules
QB/T 2614—2003
B.1α-Hu Bei The quality inspection department shall be responsible for the supervision of the production and guarantee that the new products leaving the factory meet the requirements of this standard. All non-batch products of the factory shall have a certificate, including: "name, production date, batch number, trade name, product quality certificate and standard code of this standard". 6.2 Inspection and verification The products inspected shall be in accordance with the provisions of this standard. Whether the quality meets the requirements of this note: Check once for each batch, and check separately for different batches.
6.3 The method of garbage collection is to take 2 bags of each batch of less than 100 bags, and take 336 bags of more than 1 bag in sequence, and take 50g~1K of samples from each package with a sampler, and mix the sample in the sampler, and put them into two sterilized bottles respectively: put labels on the bottles, Note: manufacturer name, product name, production date, batch number, quantity and sampling date. One bottle is for inspection and the other bottle is for storage.
6.4 If ten indicators of the acceptance set do not meet the requirements of this standard, additional samples can be taken for inspection. If there are still indicators that do not meet the requirements of the inspection results, the batch of production cannot be accepted. 6.5 When the supply and demand parties have different opinions on the product, they can reach an agreement to solve it or issue a legal control system for inspection. 7.7 Marking, packaging, transportation, and packaging 7.1 Marking Product packaging should indicate: product name, manufacturer name, trademark, batch number, net weight, lot number, and standard number: If you have special requirements before ordering, you can contact the manufacturer and make an agreement. 7.2 Packaging The product must be packed in a clean and tidy environment without any foreign objects or tin or iron wire. 2 HYY KAN KAca-QE/T 2614-2003 7.3 Transportation During transportation, the product should be loaded and unloaded carefully, and should be protected from rain and sunlight, and should comply with relevant regulations. 7.4 Storage This product should be stored in a cool, dry, ventilated warehouse to avoid foreign air pollution and away from heat sources. 7.52 If the specified storage and transportation conditions are met and the packaging is intact and not sealed, the shelf life of this product is one year: Operating conditions: Appendix A (Informative Appendix) Typical gas chromatogram of 1-amylcinnamaldehyde (hematoxylin method) Main column: Packing column, 2m~3m, inner diameter 3mm Phase: 10% PEC-20M 101 white support RO temperature: 150℃; Detector temperature: 200℃; Detector solution: Hydrogen ionization detector, carrier gas: hydrogen IfKAoNYKAa=QB/T 2614·2003
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