This standard specifies the requirements, test methods, inspection rules, marking, packaging, transportation and storage of pollution-free turbot. This standard applies to live and fresh turbot (Scophthalmus maximus Linnaeus). NY 5152-2002 Pollution-free food turbot NY5152-2002 Standard download decompression password: www.bzxz.net
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ICS67.120.30 Agricultural Industry Standard of the People's Republic of China NY 5152-—2002 Pollution-free Food Published on 2002-07-25 Turbot Implemented on 2002-09-01 Published by the Ministry of Agriculture of the People's Republic of China Market and Economic Information Department Agricultural Industry Standard of the People's Republic of China Pollution-free Food Turbot NY5152—2002 Published by China Standards Press No. 16, Sanlihe North Street, Fuxingmenwai, Beijing Postal Code: 100045||tt| |Tel: 6852394668517548 China Standards Press Printed by Huangdao Printing Factory Distributed by Beijing Xinhua Bookstore Sold by Xinhua Bookstores in various places Format 880×12301/16 Printing Sheet 1/2 Word Count 10,000 Words First Edition August 2002 First Printing August 2002 Print Quantity 1-3000 Book Number: 155066+2-14635 Price 6.00 yuan Website bzcbs.com Copyright Exclusive Infringements Must be Investigated Report Telephone: (010) 68533533 This standard was proposed by the Ministry of Agriculture of the People's Republic of China. Foreword This standard is under the jurisdiction of the National Technical Committee for Standardization of Aquatic Products. The drafting unit of this standard: National Aquatic Product Quality Supervision and Inspection Center. The main drafters of this standard are: Wang Lianzhu, Li Xiaochuan, Chen Yuanhui, Leng Kailiang, Li Zhaoxin, Zhou Deqing. NY5152—2002 1 Scope Pollution-free food turbot NY5152-2002 This standard specifies the requirements, test methods, inspection rules, marking, packaging, transportation and storage of pollution-free food turbot. This standard applies to live and fresh turbot (scophthaimus marimus Linnaeus). 2 Normative references The clauses in the following documents become the clauses of this standard through reference in this standard. For any dated referenced document, all subsequent amendments (excluding errata) or revisions are not applicable to this standard. However, the parties to the agreement based on this standard are encouraged to study whether the latest versions of these documents can be used. For any undated referenced document, the latest version shall apply to this standard. Microbiological examination of food hygienewww.bzxz.net GB 4789.4 GB 4789.7 GB4789.20 Microbiological examination of food hygiene Microbiological examination of food hygiene Microbiological examination of food hygiene Microbiological examination of food hygiene Salmonella examination Escherichia coli examination for diarrhea Vibrio parahaemolyticus examination Microbiological examination of food hygiene Aquatic food inspection GB/T5009.12 GB/T5009.15 GB/T5009.17 GB/T 5009.45- NY5029—2001 NY5070 Determination method of lead in food Determination method of pot in food Determination method of total mercury in food -1996Analytical methods of hygienic standards for aquatic productsPork of pollution-free food Pollution-free foodLimits of residues of fishery drugs in aquatic productsSC/T3303—1997 Frozen grilled eel SN0208 SN0530 3 Requirements Determination method of residues of ten sulfonamides in exported meatDetermination method of residues of thiazolidone in exported meatLiquid chromatography3.1 Sensory requirements The sensory requirements for turbot are shown in Table 1. Table 1 Sensory requirements 3.2 Safety indicators Safety indicators of turbot are shown in Table 2. Well-proportioned, normal in shape, without deformity; a small amount of white spots are allowed. The carp silk is clear, bright red or purple, the mucus is transparent, the eyeballs are full, and the cornea is clear It has the inherent fresh smell of fresh fish, no peculiar smell and is elastic NY5152-2002 Inorganic (as As)/(mg/kg) Mercury (as Hg)/(mg/kg) Lead (as Pb)/(mg/kg) (as Cd)/(mg/kg) Oxytetracycline/(mg/kg)||t t||Sulfonamides (total amount)/(mg/kg) Furazolidone Salmonella Escherichia coli Vibrio parahaemolyticus Test method Table 2 Safety index Not detectable Not detectable Not detectable Not detectable 4.1 Sensory test 4.1.1 In a well-lit and odor-free environment, place the sample on a white sugar porcelain plate or a stainless steel workbench for sensory test. When it is difficult to determine the product quality through sensory test. Perform a boiling test. 4.1.2 Boiling test: Add 500mL of drinking water to a container, boil the water, take about 100mL of fish washed with clean water, cut into pieces (no larger than 3cm×3cm), put in a container, cover, boil for 5 minutes, open the cover, smell the odor, and taste the meat. 4.2 Determination of inorganic arsenic According to the provisions of 4.5 of GB/T5009.45-1996. 4.3 Determination of mercury According to the provisions of GB/T5009.17. 4.4 Determination of lead According to the provisions of GB/T5009.12. 4.5 Determination of cadmium According to the provisions of GB/T5009.15. 4.6 Determination of oxytetracycline According to the provisions of Appendix A of SC/T3303-1997. 4.7 Determination of chloramphenicol The screening method for chloramphenicol residue shall be carried out in accordance with the provisions of Appendix A of NY5070-2002. For those with positive oxyamphenicol, the determination of its residue shall be carried out in accordance with the provisions of Appendix D (gas chromatography) of NY5029-2001. 4.8 Determination of sulfonamides The determination of sulfamethazine and sulfadimethazine in sulfonamides shall be carried out in accordance with the provisions of C5 of SC/T3303-1997, and other sulfonamides shall be carried out in accordance with the provisions of SN0208. 4.9 Determination of furazolidone Carry out in accordance with the provisions of SN0530. 4.10 Salmonella test Carry out in accordance with the provisions of GB4789.4. 4.11 Diarrhea-causing Escherichia coli test Carry out in accordance with the provisions of GB4789.6. 4.12 Vibrio parahaemolyticus test Perform according to the provisions of GB4789.7. 5 Inspection rules 5.1 Batch rules and sampling methods NY 5152—2002 5.1.1 Batch rules Live turbot is a test batch of products with the same culture conditions in the same fish pond or farm; fresh turbot is a test batch of products with the same source and size. 5.1.2 Sampling method Randomly select 5 to 10 products from each batch for sensory inspection. Randomly select at least 3 products from each batch for safety index inspection. The sampling of samples for microbiological inspection shall comply with the provisions of GB4789:1. 5.1.3 Sample preparation 5.1.3.1 Samples for safety index inspection: Take at least 3 turbots and clean them: remove the head, bones and internal organs, take the edible parts such as muscles, mince and mix them evenly and set aside: the sample volume is 400g, divided into two parts, one for inspection and the other as a reserved sample. 5.1.3.2 Samples for microbiological inspection: follow the provisions of GB4789.20. 5.2 Inspection classification Products are divided into factory inspection and type inspection. 5.2.1 Factory inspection Each batch of products shall be subject to factory inspection. Factory inspection is carried out by the producer, and the inspection items are sensory. 5.2.2 Type inspection Type inspection shall be carried out in any of the following situations. The inspection items are all the items specified in this standard. a) Turbot cultured in newly built farms: b) When the conditions for turbot culture change, which may affect product quality: c) When the national quality supervision agency proposes a type inspection requirement: d) During normal production, periodic inspection at least once a year. 5.3 Judgment rules 5.3.1 Sensory inspection of live and fresh products All inspection items shall comply with 3.1 stipulates; if two or more indicators in the test results are unqualified, it will be judged as unqualified; if one indicator is unqualified, re-sampling and re-inspection are allowed. If there are still unqualified items, it will be judged as unqualified. 5.3.2 If one indicator in the test results of the safety indicators is unqualified, the current batch of products will be judged as unqualified and shall not be re-inspected. 6 Marking, packaging, transportation, storage 6.1 Marking The name of the product, the producer and the date of manufacture shall be indicated. 6.2 Packaging 6.2.1 Packaging materials The packaging materials used shall be strong, clean, non-toxic and odorless. 6.2.2 Packaging requirements 6.2.2.1 Live turbot Sufficient oxygen shall be ensured in the packaging of live turbot. 6.2.2.2 Fresh turbot Fresh turbot should be placed in clean fish boxes or heat-insulated fish boxes: a layer of ice should be laid on the bottom of the box before placing it, and enough crushed ice should be scattered in the box to keep the fish body temperature between 0℃ and 4℃: avoid trampling or damaging the fish body with sharp objects to ensure the freshness and integrity of the fish. 6.3 Transportation 6.3.1 During the transportation of live turbot, sufficient oxygen should be ensured. 6.3.2 Fresh turbot should be transported by refrigerated or heat-insulated vehicles and ships: keep the fish body temperature between 0℃ and 4℃C. 6.3.3 The transportation vehicle should be clean and hygienic, without peculiar smell, and prevent sun exposure, pollution from pests and harmful substances during transportation, and should not be close to or in contact with corrosive substances. 6.4 Storage 6.4.1 Live turbot should be stored with sufficient oxygen. 6.4.2 Fresh turbot should be stored at a temperature between 0℃ and 4℃. 6.4.3 Products should be stored in a clean, sanitary, odor-free warehouse with rodent and insect-proof equipment to prevent contamination by insect pests and harmful substances and other damage. 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