This standard specifies the technical requirements, test methods and inspection rules for the synthesis of cinnamyl alcohol. This standard applies to cinnamyl alcohol synthesized from cinnamaldehyde by reduction reaction. QB 1783-1993 Synthetic cinnamyl alcohol QB1783-1993 Standard download decompression password: www.bzxz.net

Industry Standard of the People's Republic of China
QB1769~-1801-93
Spice Standard
(Product Standard)
Published on April 29, 1993
Implementation on December 1, 1993
Published by the Ministry of Light Industry of the People's Republic of China
1 Subject Research and Applicable Scope
Industry Standard of the People's Republic of China
Synthetic Cinnamyl Alcohol
QB1783-93
This standard specifies the technical requirements, test methods and inspection regulations for the synthesis of cinnamyl alcohol. This standard is not applicable to the following alcohols synthesized from meat aldehyde silk: 2 Reference standards
GU/T4454.% Re-feeding free-range test method
GB/T14451+2 Heat determination of aroma
CH/T14464.≥2 Determination of dehydration density
H2T14454.1 Determination of freezing point of spices
CR/T11454.17 Reference value and basic chemical composition 6T14457. Determination of the content of primary or secondary alcohol in the raw materials and synthetic materials G/T14?. Determination of the degree of decomposition of 53% of the raw materials in the raw materials and synthetic materials. General method for color analysis 3 Product chemical name, molecular formula, structural formula, molecular weight Chemical name β-aminobutyric acid alcohol
Molecular formula C, HU
Molecular weight
4 Technical requirements
CI -CHCH, OH
1318 (19th century)
4.1 Appearance: slightly yellow liquid or colorless, color not exceeding the standard color No. 10. 4.2 Odor and fragrance.
4.3 Drop point (0)
4.5 Free formaldehyde (in terms of graph) (%)
4.6 Dosage (volume)
4.7 Solubility (%)
5 Test method
5.1 Package connection
Negative reaction.
1g test file 7u (V) 1m
Ministry of Light Industry of the People's Republic of China, approved on April 29, 1993, second edition, 1993-*2-01
RGB/T14454.8
5.2 Evaluation of aroma
QG/T14454.2.
5.3 Determination of freezing point
See GB/T 14454.7.
5.4 Determination of solvent content
HGB/T 14457.6.
Note: For the determination of gas color, see GB/T 14454-14457.6.
5.5 For the determination of free aldehyde (calculated as carboxyaldehyde), see CB/T 14454-17.
5.6 Determination of microorganisms.
See G/T14454,2 (New)
5.7 Melting temperature: 25℃
EUB/T 144Y.1.
6 Inspection rules
QB1783-93
6.1 Each batch of finished products shall be inspected by the inspection department of the manufacturer: the manufacturer shall ensure that all products shipped out of the factory meet the requirements of this standard. Each product shall be issued with a quality certificate, which shall include: manufacturer name, product name, trademark, factory average daily average, batch number, license number, product quality certificate and standard abbreviation. 8.2 The acceptance unit shall carry out inspection in accordance with the provisions of this standard. Once the received product meets the requirements of this standard, it shall be inspected once more for each batch, and the batch number shall be inspected separately. 6.3 The packaging unit of each batch shall be in a drum if it is less than 100, and in three drums if it is more than 100. When sampling from non-store packages, check the appearance for moisture and quality, then shake it thoroughly and evenly, then use an effective sampling tube to absorb 5 (1mm) liquid from each vehicle. Note: The sample must be taken by the person in charge and the person in charge shall be separately inspected. Note: manufacturer name, product name, batch number, date of entry, shipping number and sampling information, and keep the same for future reference. 64. If one of the indicators of the product does not meet the requirements after the inspection, the new sample shall be taken together with the production team for analysis. If there is still any unqualified result, the product cannot be accepted. B.5 When the accepting party has any dispute with the product, it may invite the statutory inspection member to carry out the inspection and the cost shall be borne by the accepting party.
6.B Color, aroma, freezing point and free formaldehyde are the inspection indicators. Contains alcohol, oxygen and will be the new type inspection indicators, and the degree of pregnancy will be checked once every time.
7 Marking, packaging, transportation, storage
7.1 The synthetic cinnamon reduction lead barrel and the outer packaging shall be marked with the product name, manufacturer's name, trademark, batch size, net weight, tare weight, ex-factory date, system number and relevant installation marks. Order form and special requirements: according to the production, make a separate agreement, .2 During transportation, it should be protected from rain and air pollution, and strictly avoid acid, toxicity and other temperature. 3 The product should be stored in a dry, ventilated, cool place. To prevent technical pollution, these two requirements are in place, 4 In accordance with the regulations, the packaging is complete, and the product has a shelf life of one year without unauthorized use. 2
QB1783-93
Appendix A
Determination of cinnamyl alcohol content
Gas chromatography internal normalization method
(Monitoring documents)
People 7,! Color only, see only and micro-processing according to the provisions of Chapter 5 of GB1[539
Fill in length-, internal 34. www.bzxz.net
Western phase EG20M, 8%-11% lower
ChruuleBorh WAW DMCsBi~uH upper
A1.3 detector
level flame ionization detector.
A2 probe
A2, degree
protective chemical rise blue to ~,
build density R/min.
Select port, 20#.
Detector 2 core
A2,2 Clear
Carrier gas oxygen, 25ml/min
A3 Determination of chemical performance
A3.1 Chemical performance test
According to GB11539 No. 10. The test should meet the requirements,
A3.2 Note: The test method should be in accordance with GB1153 No. 11.3. The test method should be in accordance with GB1153 No. 11.4. The test results should be in accordance with GB1153 No. 11.5. The test results should be in accordance with GB1153 No. 11.6. The test results should be in accordance with GB1153 No. 11.7. The test results should be in accordance with GB1153 No. 11.8. The test results should be in accordance with GB1153 No. 11.9. The test results should be in accordance with GB1153 No. 11.10. - 63 --
Additional Notes:
QB1783-93
This standard is issued by the Quality Standards Department of the Ministry of Light Industry: This standard is under the jurisdiction of the National Seasonal Food Standardization Center. This standard is drafted by the Shanghai Spice Factory.
Drafter of this standard: Luo Jian.
This standard adopts the national standard E04V.28. Since the beginning of this standard, the original light industry standard 2-81 is used. - 64
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