HG/T 2743.3-1996 Specification for the preparation of pesticide compound powder product standards
Some standard content:
HG/T2743.3—1996
The compound preparations scientifically mixed with different pesticides can greatly improve the efficacy, reduce toxicity and delay the emergence of resistance. Therefore, the development and application of compound preparations of pesticides are important ways to use pesticides rationally and effectively prevent and eliminate diseases, insects and weeds. At present, there are hundreds of compound preparations of pesticides in my country, but many varieties lack scientific experimental basis. The preparation of compound preparation standards is mostly chaotic and of varying levels. In order to standardize the preparation format of pesticide compound preparations and improve the standard level, this standard is formulated on the basis of GB/T1.1-1993 "Guidelines for Standardization Work Unit 1: Drafting and Expression Rules of Standards Part 1: Basic Provisions for Standard Preparation" and the industry standard ZBG23001--86 "Principles and Procedures for Naming Common Names of Pesticides" of the Ministry of Chemical Industry, and on the basis of HG/T2467 "Format for Preparation of Pesticide Product Standards". Appendix A of this standard is the appendix of the standard.
This standard is proposed by the Technical Supervision Department of the Ministry of Chemical Industry of the People's Republic of China. This standard is under the jurisdiction of Shenyang Chemical Research Institute of the Ministry of Chemical Industry. This standard was drafted by Shenyang Chemical Research Institute of the Ministry of Chemical Industry. The main drafters of this standard are: Hou Yukai, Wang Xuecheng, Lou Shaowei, Yang Jian, Zhao Xinxin. bzxZ.net
HG/T2743.3—1996
Contents that should be included in the preface of pesticide compound preparation product standards 1. Special part information
The number and degree of adoption of international standards or foreign advanced standards, the differences and reasons with the adopted standards; the purpose and basis of standard drafting: the test comparison results of the toxicity, toxicity and efficacy of the compound preparation and the active ingredients of the compound preparation should be provided, and the degree of improvement in efficacy and reduction in toxicity of the compound preparation should be explained; for revised standards, the key points of revision should be explained; - Requirements for the transition period of standard implementation: the explanation that this standard leads to the abolition or replacement of all or part of other standard documents; - Indication of which appendices are standard appendices and which are indicative appendices. 2. Basic part information
This standard is proposed by...
This standard is under the jurisdiction of...
Drafting unit of this standard: When necessary, the responsible drafting unit and participating drafting units may be specified. Main drafters of this standard: Generally no more than 5 people. 300
Chemical Industry Standard of the People's Republic of China
Specification for the preparation of pesticide compound powder product standards HG/T2743.3--1996
This standard specifies the specification for the preparation of pesticide compound powder product standards, and is applicable to the preparation of corresponding national standards, industry standards, local standards and enterprise standards for pesticide compound powder products. Other names, structural formulas and basic physicochemical parameters of each active ingredient in this product are as follows: a) * (Generic name of active ingredient 1)
ISO Generic Name:
Trade Name:
CIPAC Digital Code:
Chemical Name:
Structural Formula:
Empirical Formula:
Relative Molecular Mass (Calculated by 19×× International Relative Atomic Mass): Biological Activity · (Insecticidal, Acaricidal, Bactericidal, Herbicidal) Melting Point · *℃
Boiling Point ℃
Vapor Pressure (20℃).·Pa
Solubility (g/L, 20℃):
Stability: (Stability to acid, alkali, light, heat, etc., half-life) b) · (Generic name of active ingredient 2)
Contents are the same as a.
c). (Generic name of active ingredient 3)
Contents are the same as a.
1 Scope
This standard specifies the requirements, test methods, and marking, labeling, packaging, storage and transportation of ... (name of compound preparation) powder. This standard applies to ... (name of compound preparation) powder processed from · (generic name of active ingredient 1), ·· (generic name of active ingredient 2), ··· (generic name of active ingredient 3) technical materials, fillers and necessary auxiliary agents that meet the standard. 2 Referenced standards
The provisions contained in the following standards constitute the provisions of this standard through reference in this standard. When this standard is published, the versions shown are valid. All standards will be revised, and all parties using this standard should explore the possibility of using the latest versions of the following standards. The order of arrangement of referenced standards is domestic first and then foreign. Standards at all levels should be arranged step by step, with national standards first and then industry standards; standards at the same level are arranged in the order of standard numbers; standards in different industries are arranged in alphabetical order according to the code number. GB/T1600—79 (89), Determination of moisture content in pesticides GB/T1601-93 Determination of pH value in pesticides
GB/T16041995 Acceptance rules for commercial pesticides Approved by the Ministry of Chemical Industry of the People's Republic of China on April 8, 1996, and implemented on September 1, 1996
HG/T 2743. 3—1996
GB/T1605-79 (89) Sampling methods for commercial pesticides GB3796—83 General rules for pesticide packaging
GB/T16150-1995 Method for determining the fineness of pesticide powders and wettable powders HG/T246793 Format for writing pesticide product standards HG/T2743.1—1996 Specification for writing pesticide compound emulsifiable concentrate product standards ZBG23001—86 Principles and procedures for naming common names of pesticides 3 Requirements
3.1 Appearance: It should be a free-flowing powder without lumps. 3.2. (Name of compound preparation) Powders should meet the requirements of Table 1. Table 1 (Name of compound preparation) Powder control items Index item
(Content of common name of active ingredient 1, %
(Content of common name of active ingredient 2), %
·(Content of common name of active ingredient 3), %(Content of harmful impurities), %
Moisture, %
pH range
Suspension rate, %
Fineness (passing 75μm test sieve), %
Hot storage stability|| tt||(or specified range)
(or specified range)
(or specified range)
1 The listed items are not exhaustive, nor are they required to be included in all pesticide compound powder standards. They can be increased or decreased according to the specific conditions of different pesticide compound products.
2 Hot storage stability test, at least once every month. 4 Test method
4.1 Sampling
According to GB/T1605 The method of "sampling of powders and wettable powders" in the standard is used. The sampling packages are determined by the random number table method; the final sampling volume should generally be no less than 250g.
4.2 Identification test
Write in accordance with 4.2 of HG/T2743.1 (the active ingredient should be extracted before the identification test). ·Determination of the content of (generic name of active ingredient 1) 4.3
Write in accordance with the same determination method format as HG/T2467 and this standard. 4.4·Determination of the content of (generic name of active ingredient 2) Written in accordance with the same determination method format as HG/T2467 and this standard. 4.5Determination of the content of (generic name of active ingredient 3) Written in accordance with the same determination method format as HG/T2467 and this standard. 302
4.6·Determination of the content of (name of harmful impurities) Written according to the specific determination method adopted.
4.7Determination of moisture
HG/T 2743. 3--1996
Perform according to the azeotropic distillation method in GB/T1600. 4.8 Determination of pH value
Perform according to GB/T1601.
4. 9 Determination of fineness
Perform according to the dry sieving method in GB/T16150 (if the sample is moist, it can be dried). 4.10 Hot storage stability test
4.10.1 Method summary
Through the pressurized hot storage test, the product is aged rapidly and the changes in the performance of the product stored at room temperature are predicted. 4.10.2 Apparatus
Beaker: 250mL, inner diameter 6.0~6.5cm; disc: The diameter should match the beaker and produce The average pressure is 2.45 kPa. 4.10.3 Test steps
Put 20g of sample into a beaker without any pressure, so that it can be spread into a smooth and uniform layer of equal thickness. Press the disc on the sample, put the beaker in the oven, store it at ℃ for d, take out the beaker, take out the disc, put it in the desiccator, let the sample cool to room temperature, and complete the determination of the active ingredient content and other items within 24 hours (when writing specific product standards, the judgment principle of accelerated storage test qualification should be specified). 4.11 Product inspection and acceptance
Should comply with the relevant provisions of GB/T1604. The rounded value comparison method is used for the processing of limit values. 5 Marking, labeling, packaging, purchase and transportation
.·Name of compound preparation) The marking, labeling and packaging of powders shall comply with the relevant provisions of GB3796, and shall have a production license (production permit) number and trademark.
5.2 Prepare the package based on the specific packaging regulations of each production and processing plant. 5.3 Other forms of packaging may be used according to user requirements or order agreements, but they must comply with the relevant provisions of GB3796. 5.4 Packages should be stored in ventilated and dry warehouses. 5.5 During storage and transportation, strictly prevent moisture and sunlight, do not mix with food, seeds, and feed, avoid contact with skin and eyes, and prevent inhalation through the mouth and nose. 5.6 Safety: In addition to the eye-catching toxicity mark, the instructions for use or packaging containers should also have toxicity instructions, precautions for use, symptoms of poisoning, detoxification methods and first aid measures.
5.7 Warranty period:
Under the specified storage and transportation conditions, the warranty period of ... (name of compound preparation) powder is at least two years from the date of production. During the warranty period,...
HG/T2743.3-1996
Appendix A
(Appendix to the standard)
Principles for naming common names of pesticide compound preparations According to the basic principle of ZBG23001-86 "Principles and Procedures for Naming Common Names of Pesticides" Article 1.2 "The common name of pesticide preparations (single or mixed) should include three parts, namely, the mass percentage of the active ingredient, the common name of the active ingredient and the dosage form. The common name of the mixed preparation can be composed of the prefixes or pronouns of the common names of the active ingredients". The naming of the compound preparation is divided into three parts: the first is the total content of each active ingredient in the compound preparation (mass percentage or g/L (20℃)); the second is the common name of the compound preparation, which is composed of the prefixes (or the first few characters) of the common names of each active ingredient. A dot is inserted between the prefixes (or the first few characters) to reflect the compound preparation; the order of each active ingredient should generally be determined by its content, with the higher one in front and the lower one in the back; it can also be ranked according to its contribution to the efficacy, with the one that contributes the most to the efficacy being ranked in front; the third is the dosage form of the compound preparation, such as powder, emulsifiable concentrate, wettable powder, aqueous suspension, etc. For example, 3% methyl phthalate powder, 40% dimethoate emulsifiable concentrate, 20% cypermethrin emulsifiable concentrate, 50% polysulfur suspension, etc. If a synergist is added to the compound preparation, the synergist is not counted as an active ingredient, and the proportion it occupies does not enter the total content of the active ingredients. 304
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