This standard specifies the technical requirements, test methods and inspection rules for white jasmine leaf oil. This standard applies to white jasmine leaf oil made from fresh white jasmine leaves by steam distillation in water or on water. QB/T 2239-1996 White jasmine leaf oil QB/T2239-1996 Standard download decompression password: www.bzxz.net

Light Industry Industry Standard of the People's Republic of China
QB/T 2239~2244~-96
Spice Standard
19810-11 Issued
China Light Industry Federation
1997-0701 Implementation
Light Industry Industry Standard of the People's Republic of China
Brown Orchid Leaf Oil
QB/T 2239-96
The design of this revised standard is based on the original professional standard and is implemented according to the product quality situation of the selected industry. The product quality may be affected by the influence of species, climate, etc. According to the measured data, this standard is revised at the following points: The original chemical method for measuring the content of aromatic alcohol in the sample is changed to the gas color method, which can more accurately reflect the content of aromatic alcohol.
2, the source of the alcohol is 0% (/V) technical alcohol: changed to: Appendix A in the standard.
This standard is issued by the Quality Standards Department of China Light Industry General Association. This standard is under the jurisdiction of the National Fragrance Standardization Center. The starting unit of this standard: Fujian Fragrance Cosmetics Industry Association. The main drafters of this standard are Chen Xian, Jinxiu County, Hangzhou, and Shimei. The implementation of this standard is based on the professional standard ZTY4-6 issued by the Ministry of Light Industry of the People's Republic of China. This standard defines the technical requirements for white orchid leaf oil. Test methods and test period are included. Q8/T 2239.-16
This standard applies to orchid oil with orchid freshness as raw material: orchid oil prepared by steaming in water: 2 Reference standards
The provisions contained in the underlined standards shall become the provisions of this standard through the use of this standard. This standard is effective for the versions shown: All standards will be considered, and the parties using the standards should explore the possibility of making the following standards part of the version
GB/T 14454.1-93
GR/T [4454,2--03
G/T 14-54.3-3
GH/T I+ d—
GB/T +414,5—3
GB/T [1455,2—93
GB/T 144559. -93
GB/T [4433.403
GE/T[4455.5—93
GR/T 14455.6-9S
GR/T [4435.9--98
8 Definition
Sample preparation
Aroma evaluation
Color detection
Measurement of light intensity
Determination of phase separation
Evaluation of thickness
Determination of acidity
Determination of odor
General method for analysis by steam injection
White orchid leaf refers to the fresh white orchid obtained from the white orchid tree (Micheliaulua DC) by steam addition.
4 Technical requirements
41 Color, yellow to yellow edge color, 4.2 Aroma: only with the characteristic aroma of orchid.
4.8 Density (20/2n*C): 5.B30~3,543. .4 Optical index (20*C): 1,4550~145334.5 Optical rotation (20C) -16.C~-1136 Solubility (20°C): Tested in % (/V) ethanol h, avoid saline solution. China Library Light Industry Association 1996-10-11 approved 2
18001 real bottle
.7 Acid value,
4.,B Cool value, 32,.
QB/T229-96
4.9 Alcohol content (filling phase color-method), 270.0. 5 Test method
Unless otherwise specified, the reagents used in the test are analytical reagents and the water is distilled water. 5.1 Sample preparation
See GB/T 144...
5.2 Aroma evaluation
GB/14454.2.
5.3 Determination of color
JGB/T .4434.3.
5.4 Determination of relative density, 2℃/20℃
GGH/T 14455.4.
5.5 Determination of refractive index, 20°C
WGB/T 14454.4,
5.5 Measurement of optical rotation, 21
See Gn/T 14464.h. wwW.bzxz.Net
Determination of temperature, 20*C
See GB/T 4455.3.
5.8 Determination of acetyl value
CB/T 14455.5.
5.3 Determination of acyl value
See B/T 14455.6.
6.10 Determination of alcohol content (filled column gas standard colorimetric method) 5.10.1 Instrument
5.10.1.1 Colorimeter, recorder and microprocessor shall comply with the provisions of GB/14455. Chapter 1.
Filling: 3~4u in length, 3~4mm in inner diameter
Fixed. E2M5%0%
5.10.1.2 Detector
Ammonia flame ionization detector.
5. 10,2 Operating conditions
5. 10,2,1 Chromosome oven: program temperature, 60-200 °C, rate: 1/40 °C.
Measured value: 1°C.
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5,10. 2.2 Ionization
Carrier gas flow, trace gas 25a1./mi:.
5.10.3 Determination of efficacy
5.10.a.1 Test for potency
Q日/1:2239—96
Perform the test according to the method specified in 3.1 of (1/T:446.9) and shall comply with the fee table. 5.10.3.2 Tolerance
Perform the determination of tolerance according to the method specified in 3/T14455.92.2 and shall comply with the requirements. 5.10.4 Internal chemical method: Follow G445, Rush 1, and perform the specified method. 5.10.5 Reproduction and station performance
Perform the test according to the provisions of G/141, 9, 114, and the provisions of the warehouse shall be carried out by the gas chromatogram of the Chinese Academy of Sciences. See the attached (note for caution). 6 Test specifications
6.1 The manufacturer guarantees that the products meet the requirements of technical standards. Each batch of products is accompanied by a quality certificate, including: manufacturer name, product name, trademark, production date, batch number, net weight, product compliance certificate and product number. 6.2 The acceptance unit has the right to inspect whether the products meet the requirements of the standard. One batch is selected for one acceptance, and no separate acceptance is required.
8.8 Sampling method: G3/T: 4455.2, the minimum volume of the product is 1mL. Each packaging unit is discarded: less than 200 pieces, more than 200 pieces Take two samples of 1ce oil. Take 0~[ccm3mL with a sample tube, mix all the white oil samples in a sampler, take 50~1cm3 of them and put them into a blue glass bottle, and then put them into a blue glass bottle. The name of the manufacturer, product name, number of samples and sampling date. "Bottle inspection, service: keep them separately. 64 If one of the measures in the acceptance results does not meet the requirements of this standard, the production department will re-examine the samples from the 2 times the amount of packaging together with the production department. If the re-examination results are still unqualified, the batch of products will be judged to be unqualified. 6 When the supply and demand parties have different opinions on the product, they can reach an agreement to resolve the problem. The second element is cut 7 standard, full packaging, transportation, storage
7.1 When orchid leaves are stored in a clean and odorless container or in plastic containers, the container should indicate: non-product name, product name, trademark, approval number, shipping number, tare weight, ex-factory date. If there are special requirements, the issuing unit of this standard can make an agreement with the manufacturer.
The product should be stored in a dry and ventilated warehouse to prevent pollution from foreign air and should be kept away from rain and strong winds during transportation. 7. If the product is stored in accordance with the specified conditions, the packaging is intact and it is not opened, the shelf life of this product is one year. Appendix A (for reference)
Determination of aromatic alcohol content in orchid leaf oil
Gas chromatography
Su Zhang Calculation
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