Some standard content:
1CS13.300
National Standard of the People's Republic of China
GB/T22235—2008
Determination for viscosity of liquids
Determination for viscosity of liquids Issued on 2008-06-19
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China Standardization Administration of China
Implementation on 2009-02-01
This standard is equivalent to OECD114:1981 "Determination of Viscosity of Liquids" (English version). For the convenience of use, this standard has been modified as follows: a) The "" after the chapter title number in the original standard is removed; b) The period indicated by "," in the original standard is replaced by the punctuation mark ""; Chapter 2 "Normative References" is added to this standard. This standard is proposed and managed by the National Technical Committee for the Administration of Hazardous Chemicals (SAC/TC251). GB/T22235-2008
This standard was drafted by: Sinochem Standardization Research Institute, Beijing Exit-Entry Inspection and Quarantine Bureau, Hubei Exit-Entry Inspection and Quarantine Bureau. The only drafters of this standard are: Xu Siqiao, Wang Xiaobing, Han Shen, Mei Jian, Cui Hairong, Li Jingyan, Zhou Wei, Guo Ge, Guo Jian, Zhang Junxi. This standard is published for the first time.
1 Scope
Determination of liquid viscosity
GB/T22235—2008
This standard specifies the determination method of liquid viscosity. The five methods listed in this standard are originally applicable to Newtonian fluids, among which only the rotation viscometer method can be used for non-Newtonian fluids. The specific characteristics of these methods are shown in Table 1. Table 1
Determination method
Capillary viscometer
Flow cup
Rotational viscometerwwW.bzxz.Net
Falling ball viscometer
Pulling ball viscometer
Dynamic viscosity/
(mPa·s)
Kinematic viscosity/
(mm-s)
This standard is applicable to the determination of liquid viscosity. 2 Normative references
Measurement range/
(mPa-s or mms)
Standard source
ISO3104
ISO3105
ISO3218.2
DIN53015
DIN52007.2
Temperature requirements/
The clauses in the following documents become the clauses of this standard through reference in this standard. For any dated referenced document, all subsequent amendments (excluding errata) or revisions are not applicable to this standard. However, the parties to an agreement based on this standard are encouraged to study whether the latest versions of these documents can be used. For any undated referenced document, the latest version applies to this standard. ISO3104 Petroleum products Determination of kinematic viscosity of transparent and opaque petroleum liquids and calculation of dynamic viscosity ISO3105 Specifications and operating instructions for glass capillary kinematic viscometer ISO3218.2 Naming principles for essential oils
ISO3219:1977 Test methods for precious metal pastes for thick film microelectronics Determination of viscosity ASTMD-88-56 Test method for Saybolt viscosity ASTMD-914.25-37 Test method for ethyl fiber ASTMD-562-55 Test method for determination of consistency of coatings by Stirling viscometer ASTMD-1200-70 Test method for determination of viscosity by Ford viscosity cup ASTMD2392 Test method for color of pigmented aviation gasoline ASTMD2983 Test method for low temperature viscosity of automotive liquid lubricants by Brookfield rotary viscometer ASTMD3 346-74 Test methods for rubber properties Determination of the processability of SBR (styrene-butadiene rubber) using a Mohs viscometer DIN51366 Inspection of mineral oil hydrocarbons Measurement of the kinematic viscosity of opaque liquids using the Cannon-Fenske viscometer DIN51377
DIN51398
DIN51550
Lubricant inspection Determination of the viscosity of engine lubricating oils at low temperatures using a cold start simulator Lubricant inspection Determination of the apparent viscosity at low temperatures using a Brookfield viscometer (liquid bath method) Viscosity measurement Determination of viscosity General principles
Mineral oil inspection Inspection of liquid fuels and related liquids Determination of viscosity using the Vogel-Ossng viscometer Viscosity stability range DIN51561
: approximately 10-150°C (139)
DIN 51562.1
Viscosity measurement
Measurement of kinematic viscosity with Ubber-lahde viscometerMicro Ubbelohde viscometerDIN 52007.2
Testing of asphalt adhesivesViscosity determination with a ball viscometerGB/T22235—2008
DIN52312.2Testing of glassViscosity measurement with a rotational viscometerDIN53015Viscosity measurement with a Hoeppler falling ball viscometerDIN53019.1Viscosity measurementViscosity and flow line measurement with a rotational viscometer of standard geometry and structureDIN53177 Adhesives for paints and coatingsDynamic viscosity of liquid resins, resin solvents and oils measured with a capillary viscometer according to the Ubbelohde method.
DIN53214 Inspection of coatings Determination of flow rate curve and viscosity using a rotational viscometer DIN53229 Determination of viscosity at high speed drop using a rotational viscometer for paints, coatings and similar coating materials DIN53921 Determination of fluidity using a rotational viscometer for surfactants (IDTISO6388:1989) 3 Terms and definitions
The following terms and definitions apply to this standard. 3.1
Viscosity
Also known as viscosity or internal friction, is a property of a fluid that hinders its relative motion, that is, the property of a liquid substance under stress when it is deformed. It depends on the rate of deformation, and stress can also be considered as the cause of the deformation rate. The relationship between tangential force and tangential velocity D is shown in the following formula:
will be defined as dynamic viscosity.
For Newtonian fluids, the viscosity is a constant at all tangential velocities, and its magnitude is determined by pressure and temperature. For non-Newtonian fluids, the viscosity changes with the change of tangential velocity. If the viscosity is measured by a capillary viscometer without applying external pressure, the measured value is the ratio of dynamic viscosity to density, which is kinematic viscosity. The SI unit of dynamic viscosity is Pa·s, and the more suitable unit in actual use is mPa·s. The conversion relationship between them is: 1 mPa·s= 10* Pa.s
The S unit of kinematic viscosity is m*/s1mm/s=10-m/s4Required information
Required information is as follows:
a) Density (for falling ball viscometer method); b) Melting point/melting temperature range of amorphous materials; c) Boiling point/boiling temperature range.
5Reference materials
The following reference materials are mainly used to calibrate methods and compare when applying another method. When studying new chemical substances, reference materials are not required in all cases. The reference materials are shown in Table 2. Table 2 Reference list (from IUPAC)\Chemical name
Identification value and precision
Mineral oil series (classified,
20℃.C1~2.7)×10mPa.s (1.25×10t part is natural, part
is a relative)
JS2.5-2000 type (including
10 kinds of products)
mm/s), error ±0.2%, ±0.3% at 4000mPa-s
The range of the signed dynamic viscosity (mPa·s) and kinematic viscosity (mm/s) is 2~1800 (20℃)
6×10 *mm2/s(20℃)
2X10°mm/s(20C)
Newton fluid, measured by capillary viscometer Bellaud viscometer with suspension surface, also has data for other temperatures (20~100℃)
Chemical name
Mineral oil
Mineral oil
Polyisobutylene
11 mineral oil series
7 polyisobutylene series
Identification value and accuracy
Table 2 (continued)
(11~1000)mPa*5,±0.1%(20C)
(10~10*)mPa*$,±0. 5%(20 )
(10*~105)mPa- $,±1. 5%(20 C) Identification viscosity range 1.503±0.1%~1720±0.2%mPas(20)
Identification viscosity range 4170±1.3%~5.89×10±1.0%mPa-s(20)
“The units used in the table are based on the original report of the laboratory that published the data. Source”
GB/T22235—2008
Newtonian fluids, density and kinematic viscosity were also determined. Newtonian fluids, kinematic viscosity and density were determined using the rotational viscometer method. There are also data at 50°C and 80°C.
There are also data at 50°C, 80°C and 100°C.
bThe reporting country and institution address are as follows:
CGermanyThe Pysikalische-Technische Bundesanstalt 33 Braunschwelg,Bundesallee 1oo,Federal Republieof Germany.
E-JapanNational Chemical Laboratory for Industry,Ministry of International Trade & Industry,l-1Hommachi,ShibuyakuTokyo,15l,Japan.DHungarianNationalOfficeofMeasuresNemetolgylut37-39,SZ,BudapestXIIHungaryGPolishDivisionofPhysical-ChemicalMetrology,NationalBoardforQualityControlandMeasures-2,ElektoralnaStreet,Warsaw,Poland.6Principle
Viscosity can be measured according to the following three measurement principles: the liquid to be measured flows through a capillary tube - capillary viscometer or flow cup; a)
Liquid shears between concentric cylinders, conical plates and parallel plates - rotational viscometer method; c) Dynamic viscosity is measured by the movement of a small ball in a cylinder vertically or obliquely filled with liquid - Hopple falling ball viscometer, pulling ball viscometer, etc.
When using the Hopple viscometer, the density should be known first to calculate the dynamic viscosity. 7 Test steps
7.1 Apparatus
7.1.1 The design of capillary viscometers is described in the following standard documents: ISO3104, ISO3105DIN51550.DIN51562.1DIN51561.DIN51366.DIN53177, ASTMD-1200-70, ASTMD-2392.ASTMD-914.25-37.ASTMD-88-56. 7.1.2 The design and use principle of standard rotational viscometers are almost without exception only related to the flow state of the liquid, the magnitude of the shear force, the velocity gradient and the type of substance. The detailed information is described in the following documents: ISO3219:1977.DIN51398, DIN51377DIN53214, DIN53019.1.DIN53229, DIN 52312.2, DIN53921, ASTMD-562-55. ASTMD-3346-74. ASTMD-2983.
7.1.3 The design and use of the force ball viscometer are only standardized in some national standards, such as DIN53015, DIN52007.2 and ASTMD-914.25-37
7.2 Test conditions
The viscosity measurement should be carried out at a constant temperature, preferably at 20°C or a temperature slightly above 20°C. At least 2 tests should be conducted at each temperature.
7.3 Test operation
The measurement should be carried out according to the provisions of each standard. 3
GB/T22235-2008
3 Data processing and test report
8.1 Data processing
The viscosity shall be measured according to the relevant standards of capillary viscometer and force ball viscometer. Rotational viscometer is only applicable to Newtonian fluids; for non-Newtonian fluids, it is assumed that they conform to the laws of Newtonian fluids, and the measured results are expressed in the form of flow curves. At the same time, the curves obtained by the rotational viscometer test shall be calculated and explained. In addition, the test errors shall be discussed according to the standard requirements of capillary viscometer, force ball viscometer and rotational viscometer.
8.2 Test report
Write the experimental report according to the test report writing regulations of each standard. The report shall include the individual measured values and the average value at each temperature. And the differences from the standard method in the test steps shall be detailed. References
GB/T22235—2008
[1] IUPAC, Physicochemical Measurements: Catalog of Reference Materials fromNational Laboratories,in:Pure and Applied Chemistry,Pergamon Press,1976,48:513-514[2] W. Wazer,JW Lyons,KJ Kim and RE Kolwell, Viscosity and Flow Measurement,Laboratory Handbook of R heology,Inst.Publ.New York-London,l963GB/T22235-2008
People's Republic of China
National Standard
Determination of Liquid Viscosity
GB/T22235-2008
Published and distributed by China Standards Promotion Publishing House
No.16,Sanlihebei Street, Fuxingmenwai, Beijing
Postal Code: 100045
Website:spe.net.cn
68517548||tt| |Tel: 68523946
Printed by China Standard Press, Thailand Royal Island Printing Factory, distributed by Xinhua Bookstores in various places
Format 880×12301/16
Printing sheet 0.T5 Word count 9,000 words
First edition in September 2008 First printing in September 2008 Book number: 155066-1-33358 Price 14.00 yuan If there is any printing error, our distribution center will replace it. Copyright infringement will be investigated
Report telephone: (010) 685335336 Principles
Viscosity can be measured according to the following three measurement principles: the liquid to be measured flows through a capillary tube - capillary viscometer or flow cup; a)
The liquid is sheared between concentric cylinders, conical plates and parallel plates - rotational viscometer method; c) The dynamic viscosity is measured by the movement of a small ball in a cylinder filled with liquid vertically or obliquely - Hopple falling ball viscometer, pulling ball viscometer, etc.
When using the Hopple viscometer, the density should be known first to calculate the dynamic viscosity. 7 Test steps
7.1 Apparatus
7.1.1 The design of capillary viscometers is described in the following standard documents: ISO3104, ISO3105DIN51550.DIN51562.1DIN51561.DIN51366.DIN53177, ASTMD-1200-70, ASTMD-2392.ASTMD-914.25-37.ASTMD-88-56. 7.1.2 The design and use principle of standard rotational viscometers are almost without exception only related to the flow state of the liquid, the magnitude of the shear force, the velocity gradient and the type of substance. The detailed information is described in the following documents: ISO3219:1977.DIN51398, DIN51377DIN53214, DIN53019.1.DIN53229, DIN 52312.2, DIN53921, ASTMD-562-55. ASTMD-3346-74. ASTMD-2983.
7.1.3 The design and use of the force ball viscometer are only standardized in some national standards, such as DIN53015, DIN52007.2 and ASTMD-914.25-37
7.2 Test conditions
The viscosity measurement should be carried out at a constant temperature, preferably at 20°C or a temperature slightly above 20°C. At least 2 tests should be conducted at each temperature.
7.3 Test operation
The measurement should be carried out according to the provisions of each standard. 3
GB/T22235-2008
3 Data processing and test report
8.1 Data processing
The viscosity shall be measured according to the relevant standards of capillary viscometer and force ball viscometer. Rotational viscometer is only applicable to Newtonian fluids; for non-Newtonian fluids, it is assumed that they conform to the laws of Newtonian fluids, and the measured results are expressed in the form of flow curves. At the same time, the curves obtained by the rotational viscometer test shall be calculated and explained. In addition, the test errors shall be discussed according to the standard requirements of capillary viscometer, force ball viscometer and rotational viscometer.
8.2 Test report
Write the experimental report according to the test report writing regulations of each standard. The report shall include the individual measured values and the average value at each temperature. And the differences from the standard method in the test steps shall be detailed. References
GB/T22235—2008
[1] IUPAC, Physicochemical Measurements: Catalog of Reference Materials fromNational Laboratories,in:Pure and Applied Chemistry,Pergamon Press,1976,48:513-514[2] W. Wazer,JW Lyons,KJ Kim and RE Kolwell, Viscosity and Flow Measurement,Laboratory Handbook of R heology,Inst.Publ.New York-London,l963GB/T22235-2008
People's Republic of China
National Standard
Determination of Liquid Viscosity
GB/T22235-2008
Published and distributed by China Standards Promotion Publishing House
No.16,Sanlihebei Street, Fuxingmenwai, Beijing
Postal Code: 100045
Website:spe.net.cn
68517548||tt| |Tel: 68523946
Printed by China Standard Press, Thailand Royal Island Printing Factory, distributed by Xinhua Bookstores in various places
Format 880×12301/16
Printing sheet 0.T5 Word count 9,000 words
First edition in September 2008 First printing in September 2008 Book number: 155066-1-33358 Price 14.00 yuan If there is any printing error, our distribution center will replace it. Copyright infringement will be investigated
Report telephone: (010) 685335336 Principles
Viscosity can be measured according to the following three measurement principles: the liquid to be measured flows through a capillary tube - capillary viscometer or flow cup; a)
The liquid is sheared between concentric cylinders, conical plates and parallel plates - rotational viscometer method; c) The dynamic viscosity is measured by the movement of a small ball in a cylinder filled with liquid vertically or obliquely - Hopple falling ball viscometer, pulling ball viscometer, etc.
When using the Hopple viscometer, the density should be known first to calculate the dynamic viscosity. 7 Test steps
7.1 Apparatus
7.1.1 The design of capillary viscometers is described in the following standard documents: ISO3104, ISO3105DIN51550.DIN51562.1DIN51561.DIN51366.DIN53177, ASTMD-1200-70, ASTMD-2392.ASTMD-914.25-37.ASTMD-88-56. 7.1.2 The design and use principle of standard rotational viscometers are almost without exception only related to the flow state of the liquid, the magnitude of the shear force, the velocity gradient and the type of substance. The detailed information is described in the following documents: ISO3219:1977.DIN51398, DIN51377DIN53214, DIN53019.1.DIN53229, DIN 52312.2, DIN53921, ASTMD-562-55. ASTMD-3346-74. ASTMD-2983.
7.1.3 The design and use of the force ball viscometer are only standardized in some national standards, such as DIN53015, DIN52007.2 and ASTMD-914.25-37
7.2 Test conditions
The viscosity measurement should be carried out at a constant temperature, preferably at 20°C or a temperature slightly above 20°C. At least 2 tests should be conducted at each temperature.
7.3 Test operation
The measurement should be carried out according to the provisions of each standard. 3
GB/T22235-2008
3 Data processing and test report
8.1 Data processing
The viscosity shall be measured according to the relevant standards of capillary viscometer and force ball viscometer. Rotational viscometer is only applicable to Newtonian fluids; for non-Newtonian fluids, it is assumed that they conform to the laws of Newtonian fluids, and the measured results are expressed in the form of flow curves. At the same time, the curves obtained by the rotational viscometer test shall be calculated and explained. In addition, the test errors shall be discussed according to the standard requirements of capillary viscometer, force ball viscometer and rotational viscometer.
8.2 Test report
Write the experimental report according to the test report writing regulations of each standard. The report shall include the individual measured values and the average value at each temperature. And the differences from the standard method in the test steps shall be detailed. References
GB/T22235—2008
[1] IUPAC, Physicochemical Measurements: Catalog of Reference Materials fromNational Laboratories,in:Pure and Applied Chemistry,Pergamon Press,1976,48:513-514[2] W. Wazer,JW Lyons,KJ Kim and RE Kolwell, Viscosity and Flow Measurement,Laboratory Handbook of R heology,Inst.Publ.New York-London,l963GB/T22235-2008
People's Republic of China
National Standard
Determination of Liquid Viscosity
GB/T22235-2008
Published and distributed by China Standards Promotion Publishing House
No.16,Sanlihebei Street, Fuxingmenwai, Beijing
Postal Code: 100045
Website:spe.net.cn
68517548||tt| |Tel: 68523946
Printed by China Standard Press, Thailand Royal Island Printing Factory, distributed by Xinhua Bookstores in various places
Format 880×12301/16
Printing sheet 0.T5 Word count 9,000 words
First edition in September 2008 First printing in September 2008 Book number: 155066-1-33358 Price 14.00 yuan If there is any printing error, our distribution center will replace it. Copyright infringement will be investigated
Report telephone: (010) 68533533l963GB/T22235-2008
People's Republic of China
National Standard
Determination of Liquid Viscosity
GB/T22235-2008
Published and distributed by China Standards Promotion Publishing House
No. 16, Sanlihebei Street, Fuxingmenwai, Beijing
Postal Code: 100045
Website: spe.net.cn
68517548
Tel: 68 523946
Printed by China Standard Press, Thailand Royal Island Printing Factory, distributed by Xinhua Bookstores in various places
Format 880×12301/16
Printing sheet 0.T5 Word count 9,000 words
First edition in September 2008 First printing in September 2008 Book number: 155066-1-33358 Price 14.00 yuan If there is any printing error, our distribution center will replace it. Copyright infringement will be investigated
Report phone: (010) 68533533l963GB/T22235-2008
People's Republic of China
National Standard
Determination of Liquid Viscosity
GB/T22235-2008
Published and distributed by China Standards Promotion Publishing House
No. 16, Sanlihebei Street, Fuxingmenwai, Beijing
Postal Code: 100045
Website: spe.net.cn
68517548
Tel: 68 523946
Printed by China Standard Press, Thailand Royal Island Printing Factory, distributed by Xinhua Bookstores in various places
Format 880×12301/16
Printing sheet 0.T5 Word count 9,000 words
First edition in September 2008 First printing in September 2008 Book number: 155066-1-33358 Price 14.00 yuan If there is any printing error, our distribution center will replace it. Copyright infringement will be investigated
Report phone: (010) 68533533
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