This standard specifies the technical requirements, test methods and inspection rules for ethyl propionate. This standard applies to ethyl propionate produced by chemical synthesis using propionic acid and ethyl alcohol as raw materials. This product is mainly used to prepare edible flavors. QB 1954-1994 Food Additive Ethyl Propionate QB1954-1994 Standard Download Decompression Password: www.bzxz.net
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Light Industry Industry Standard of the People's Republic of China Food Additives Ethyl Propionate 1 Subject Content and Scope of Application This standard specifies the technical requirements, test methods and inspection rules for ethyl propionate. QB1954-94 This standard applies to ethyl propionate prepared by chemical synthesis using propionic acid and ethanol as raw materials. This product is mainly used for blending edible flavors. 2 Reference Standards GB190 Dangerous Goods Packaging Marking GB11540 Determination of relative density of isolated and synthetic spices GB/T14454.2 Flavor aroma evaluation method GB/T14454.3 Flavor color test method GB/T14454.4 Determination of refractive index of spices GB/T14457.4 Determination of acid value or acid content of isolated and synthetic spices GB/T 14457.5 Determination of ester content in isolated and synthetic fragrances 3 Product chemical name, molecular formula, structural formula, molecular weight Chemical name Ethyl propionate Molecular formula: C, H1.02 Structural formula: CH—CHz Molecular weight: 102.13 (according to the international atomic weight in 1987) 4 Technical requirements Color: colorless and transparent liquid, the color does not exceed the color scale of standard colorimetric solution No. 4. 4.2. Aroma: similar to pineapple aroma. 4.3 Relative density (25/25℃): 0.885~0.889. 4.4 Refractive index (20℃): 1.383~1.385. 4.5 Acid value (mgKOH/g): ≤1.0. Ester content (%): ≥96.0. 5 Test methodsbzxZ.net Unless otherwise specified, the test materials used in the tests are analytical reagents and the urine is distilled water of the appropriate purity. 5.1 Determination of color See GB/T 14454.3. Approved by the Ministry of Light Industry of the People's Republic of China on June 10, 1994, and implemented on February 1, 1995 5.2 Evaluation of aroma See GB/T 14454.2. 5.3 Determination of relative density, 25/25℃ See GB11540. 5.4 Determination of refractive index, 20℃. See GB/T 14454, 4. 5.5 Determination of acid value See GB/T 14457.4. 5.6 Determination of ester content See GB/T14457.5. 6 Inspection rules QB1954-94 6.1 Ethyl propionate shall be inspected by the technical inspection department of the manufacturer. The manufacturer shall ensure that all products leaving the factory meet the requirements of this standard. Each batch of products leaving the factory shall be accompanied by a quality certificate, which shall include: manufacturer name, product name, production date, batch number, net weight, product quality certificate of compliance with this standard and standard number. 6.2 The acceptance unit has the right to inspect whether the quality of the received products meets the requirements of this standard in accordance with the provisions of this standard. Each batch number shall be inspected once, and different batch numbers shall be inspected separately. 6.3 For each batch of packaging units, two barrels (bottles) shall be selected for less than 100 barrels (bottles), and three barrels (bottles) shall be selected for more than 100 barrels (bottles). When opening the package for sampling, the appearance should be checked for moisture and impurities, and then shake to mix thoroughly. Then use a glass sampling tube to absorb 50-100 mL of the sample. Inject into the sample mixer and mix evenly, and put into two clean, dry glass bottles with ground stoppers. Indicate the manufacturer's name, product name, batch number, quantity and sampling date on the bottles. One bottle is used for inspection, and the other bottle is kept for reference. 6.4 If one of the indicators in the acceptance results does not meet the requirements of this standard, the manufacturer can re-examine the sample from twice the amount of packaging together with the manufacturer. If the re-examination results still show unqualified indicators, the batch of products cannot be accepted. 6.5 When the supply and demand parties have objections to the product quality, they can resolve them by agreement or by arbitration by the statutory testing agency. The cost shall be borne by the investor. 7 Marking, packaging, transportation and storage 7.1 Ethyl propionate is packed in iron barrels or glass bottles. The packaging is marked with: food additive product name, manufacturer name, batch number, net weight, tare weight, date of manufacture, this standard number and the "flammable goods" mark in GB190. If the ordering unit has special requirements, it can make a separate agreement with the manufacturer. 7.2 This product should be stored in a dry, ventilated and cool warehouse to prevent contamination by foreign air and keep away from fire sources. Transportation must comply with the regulations of relevant departments. 7.3 This product has a shelf life of one year if it meets the specified storage and transportation conditions, the packaging is intact and has not been opened. Additional instructions: This standard was proposed by the Quality Standards Department of the Ministry of Light Industry. This standard is under the jurisdiction of the National Flavor Standardization Center and the Food Hygiene Supervision and Inspection Institute of the Ministry of Health. This standard was drafted by the Flavor Industry Science Research Institute of the Ministry of Light Industry and Wujiang Edible Flavor Factory. This standard refers to the 1981 edition of the US FCC (1). The main contributors to this standard are Zhou Wengao, Yu Cuidi and Du Shixiang. Tip: This standard content only shows part of the intercepted content of the complete standard. If you need the complete standard, please go to the top to download the complete standard document for free.