Some standard content:
Preface
Article 4.3 of this standard is mandatory, and the rest are recommended. GB12953—2003 | The degree of consistency of "Requirements for Chlorinated Polyethylene (PE-C) Plastic Roofing Membranes and Plastic Sealing Membranes" is non-equivalent
The main difference between this standard and DIN16736 and DIN16737 is: the addition of no composite layer Class chlorinated polyethylene waterproofing membrane: divided into type 1 and type Ⅱ according to performance;
-L type I product has a break elongation and low temperature bending property higher than DIN16736 requirements; a W type Ⅱ product The tensile force is lower than the requirements of DIN16737, the elongation at break is expressed by the elongation between clamps, and the low bending property is higher than the requirements of DIN16737;
—the water vapor permeability coefficient is cancelled,
This standard replaces GB12953-1991 "Fluorinated Ethylene Waterproof Membrane", the main difference between this standard and GB12953-1991 is that the product models are divided into type I and type II (3.1 in the 1991 version; 3.1 in this version): 1. Added single-sided fiber seam composite , Category of reinforcing joints in fabrics (3,1 in this edition): For single-sided fiber composites and reinforced coils in fabrics, the unit width tensile force is used instead of tensile strength, and the breaking elongation between them is used instead of the breaking elongation between the marking lines. rate, the shape of the specimen was changed (5 in the 1991 edition; 5.5.3 in this edition); a pair of impermeability and adhesion test methods were adjusted, and specific requirements were given for the durability test method (1991 edition) 5; 5.10, 5.13 of this edition)
This standard was proposed by the National Building Materials Industry Bureau (formerly). This standard is under the jurisdiction of the National Technical Committee for Standardization of Lightweight and Decorative Building Materials (CSBTS/TC195). The units responsible for drafting this standard are: Suzhou Waterproof Materials Research and Design Institute of China National Chemical Building Materials Corporation, National Institute of Standardization of Building Materials Industry, and Shanghai Academy of Building Sciences. Units participating in the drafting of this standard: Changshu Sanheng Building Materials Co., Ltd., Shaoxing Rubber Co., Ltd., Wujin Waterproof Materials Factory, Shanghai Funa Special Waterproof Materials Co., Ltd., Shanghai Linhe Special Waterproof Materials Factory, Shaoxing County Tianyi Waterproof Materials Co., Ltd. Company, Heilongjiang Longguang Building Materials Co., Ltd., Wuxi Hengxing Rubber Products Co., Ltd. The main drafters of this standard are Zhu Zhiyuan, Yang Bin, Han Zhenxiong, Li Jiahao, Meng Yuezhen, Yu Zuiying, Zhu Longfei, Yang Linbo, and Xu Shuimu, and the previous standards replaced by this standard Version release status is: GB12953-1991.
1. Scope
Chlorinated polyethylene waterproofing membrane
GB12953-2003
This standard specifies the fluorination case Markings, requirements, test methods, inspection rules, markings, packaging, transportation and storage of vinyl waterproofing membranes. This standard applies to waterproofing membranes made of chlorinated polyethylene as the main raw material used in building waterproofing projects, including chlorinated polyethylene waterproofing membranes without composite layers, single-sided fiber composites and fabric-reinforced chlorinated polyethylene waterproofing membranes. 2 Normative reference documents
The provisions in the following documents become provisions of this standard through reference in this standard. For dated reference documents, all subsequent amendments (excluding corrigenda) or revisions do not apply to this standard. However, parties to an agreement based on this standard are encouraged to study whether they can use the new versions of these documents. Edition, for any undated reference documents, the new edition shall apply to this standard, GB/T328 Test Method for Asphalt Waterproofing Membranes
GB/T528-1998 Determination of Tensile Stress Strain Properties of Vulcanized Rubber or Thermoplastic Rubber ( eqvISO37: 1994) GB/T13022-1991 Plastic membrane tensile property test method GB/T18244-2000 Building waterproofing material aging test method 3 classification and labeling
3.1 classification
Products are classified according to whether they have a composite layer or not Classification: those without composite layers are classified as N type, those composited with fibers on one side are classified as L type, and those reinforced within the fabric are classified as W type. Each type of product is divided into Type I and Type III based on physical and chemical properties. 3.2 Specifications
The coil length specifications are 10m, 15m, and 20m. Thickness specifications are 1.2mm, 1.5mm, and 2.0mm. Other length and thickness specifications can be agreed upon by both parties. The thickness specification shall not be less than 1.2mm. 3.3 Mark
Mark according to product name (code name CPE membrane), exposed or non-exposed use, type, type, thickness, length x width and standard sequence. Example:
Type II type L exposed chlorinated polyethylene waterproofing membrane with a length of 20m, a depth of 1.2m, and a thickness of 1.5mm is marked as; CPE membrane exposed LI1.5/20X1.2GB12953-20034 requirements||tt ||4.1 Dimensional deviation
The length and width shall not be less than 99.5% of the specified value. See Table 1 for thickness deviation and minimum single value.
GB129532003
Thickness
Degree
1,2
1.5
2.0
4.2 Appearance
Table 1 Thickness
Permissible deviation
±0.10
±o, 15
±0.20
·
Minimum single value||tt ||1. 00
1, 30
1.70
Unit is millimeter
The joints of the rolled material should not be more than one, and the shorter section should be not less than 1.70
At 1.5m, the joints should be cut neatly and lengthened by 150mm. 1 | The physical and chemical properties of the coils should comply with the requirements in Table 2, and the coils with L-type fiber single-sided composite and W-type fabric reinforcement should comply with the requirements in Table 3. Table 2 Physical and chemical properties of type N difference materials
serial number
-
2
3
4
5
6| |tt||9
10
Tensile strength/MPa
Elongation at break/%
Dimensional change rate of heat treatment/%
Low temperature rate Foldability
Puncture resistance
Impermeability
Item
Adhesion in sheared state/(N/mm))
Appearance
Change rate of tensile strength/%
Heat aging treatment
Change rate of new crack elongation/3%6
Low temperature bending property
Tensile strength change rate/%
Chemical invasion resistance
Accelerated aging of artificial air chopsticks
Change rate of elongation at break/%
Low temperature odd folding property|| tt||Change rate of tensile strength/%
Change rate of elongation at break/%
Low temperature bending property
Note: Accelerated aging of artificial air chopsticks is not required for non-exposed use. performance. 2
Type I
5.0
200
3.0
No cracks at 20℃
Impermeable
Impermeable
Type II
8.0
300
Lead direction 2.5
Transverse direction 1.5
No cracking effect at 25℃
3,0 or the coil is acid damaged
No blistering, cracks, adhesion and hole adjustment
+50
20
+50
-30| |tt||No cracking at 15℃
± 30
±30
—No cracking at 15℃
+50
20|| tt||+50
30
-15℃ without grain
±20
±20
—20℃ without grain||tt ||±20
±20
—No cracking at 20℃
±20
±20
—No cracking at 20℃||tt| |5
Serial number
2
4
5
6
8
10
Force/(N/em)
Disruption elongation/%
Dimensional change rate of heat treatment/%
Low mix bending property
Punch-through resistance| |tt||Impermeability
Adhesion under shear
Property/(N/mm)
Thermal aging treatment
Chemical attack resistance||tt ||Artificial climate accelerates aging
item
L category
w category
Appearance
Table 3 L and W category physical and chemical properties
Tensile force/(N/em)
Elongation at break/%
Low temperature bending property
Control force/(N/em)||tt| |Elongation at break/%
Low temperature folding property
Tensile force/(N/cm)
Elongation at break/%
Low temperature folding property| |tt||Note: For non-exposed use, the artificial climate accelerated aging performance does not need to be evaluated. Test method
5.1 Standard test conditions
Temperature: (23±2)℃; Relative mixing degree: (60± 15)%. 5.2
Specimen preparation
B
Guang E
G
H
H
H||tt| |Picture 1 cutout of specimen
Type I
70
125
-20℃ no cracks
1.0
GB12953— 2003
Type II
120
250
—25℃ no cracks
Impermeable
Impermeable
3 ,0 or the coil is damaged
6.0 or the coil is acid damaged
No leakage, cysts, adhesion and pores
55
100||tt| |-15℃ no cracks
55
100
-15℃ no baby marks
55
100
15℃ no crack
1-1
1 -1
1-2
12
1-2
100
200
-20℃ no cracking effect
100
200
-20℃ no cracking
100
200||tt| |-20℃ no cracks
13
1-3
1-3
GB12953—2003
The tested sample will be tested under standard test conditions Leave it for 24 hours, and cut out the required test pieces according to Figure 1 and Table 4. The distance between the test pieces and the edge of the coil should not be less than 100mm. When cutting fabric reinforcement coils, you should follow the direction of the fabric and try to maximize the number of fibers in the working area. 5.3 Dimensional deviation
5.3.1 Use a tape measure with a minimum graduation value of 1mm to measure the width and length at 3 locations at both ends and the middle of the roll. Multiply the average length by the average width to obtain each roll. The area of ??the material. If there is a joint, it is calculated by subtracting 150mm from the sum of the measured lengths of the two sections. 5.3.2 Thickness
5.3.2.1 Thickness of N and W type coils
The graduation value for the thickness of N and W type coils is 0.01mm, the pressure is (22±5)kPa, The thickness measurement disk with a contact surface diameter of 6 mm has a holding time of 5 seconds. Measure 5 points in the width direction of the roll, and take one point inward from the edge of the label (100 ± 15) mm in the length direction. Take the remaining 3 points equally among these two points, and use the average of the 5 points as the thickness of the roll. , and report the minimum single value, 5.3.2.2L type coil thickness
Table 4 specimen size and quantity
serial number
1
2
3
4
5
6
7
8
9
5.3.2.2.1||tt ||5.3.2.2.2
item
item
tensile properties
heat treatment dimensional change rate
resistance to puncture
no Water permeability
Low temperature bending
Adhesion under shear state
Thermal aging treatment
Chemical corrosion resistance
Accelerated aging of artificial air chopsticks| |tt||symbol
A,A
c
B
D
E
G
1- 1.I-2, 1-3
H
Reading microscope: minimum graduation value 0.01mm. Dimensions (longitudinal |tt||200×300
300×200
300×200
300×200
Quantity
6 each
3
3
3
2
2
3
3 each
3
L type According to 5.3.2.1, take a 50mm × 50mm sample at each of the five points of the fiber single-sided composite membrane. Use a thin sharp blade along the width direction of each sample to cut a strip of approximately 50mm × 2mm perpendicular to the surface of the sample. Test strip, be careful not to deform the cross section of the test strip (section in the thickness direction). Place the cut surface of the test strip upward on the sample stage of the reading microscope, and read the thickness of the chlorinated vinyl layer of the roll (excluding the fiber layer). For products with embossed patterns on the surface, calculate the thickness based on the tangent position of the outermost end of the pattern. , measure 4 points on each test strip, the thickness is expressed as the average of 20 values ??from 5 test strips, and the smallest single value among the 20 points is reported. 5.4 Appearance
The appearance of the coil is inspected by visual inspection,
5.5 Tensile performance
5.5.1 Tensile testing machine
can measure the tensile force and elongation at the same time to ensure the tensile strength The test value is between 20% and 80% of the measuring range, with an accuracy of 1%; it can reach a tensile speed of (250±50) mm/min, and the length measuring device and measurement accuracy are 1mm. 5.5.2 Tensile properties of N type coils
5.5.2.1 Test steps
The test pieces are cut according to the requirements of Table 4 in Figure 1, and the type I sleeping material conforming to the provisions of 7.1 in GB/T528-1998 is used As shown in Figure 2, the specimen has a tensile speed of (250 ± 50) mm/min, a clamp spacing of about 75 mm, and a marking line distance of 25 mm. Use the thickness gauge required in 5.3.2.1 to measure the thickness of the marking line and the three middle points, and take the median value as the thickness of the specimen. Place the test piece in the center of the holder and clamp it without twisting, and start the tensile testing machine. Read the maximum tensile force P of the specimen and the length L between the marking lines when the specimen breaks. If the specimen breaks outside the marking lines, the data will be invalid and a spare specimen will be used to make up for it. A-
C
D
R-
L
5.5.2.2
Total length, minimum value 115, ||tt| |Width of gauge section 6.0+0.4;
Length of gauge section 33±2+
End width 25±1:
Large radius 25±2:||tt ||Small radius 14±1:
The distance quotient between gauge lines is 25±1.
Result calculation
c
·Figure 2N type bell-shattering test Piece
The tensile strength of the specimen is calculated according to formula (1), accurate to 0.1MPa: TS-P/(BXd)
Where:
TS-
P
B
Tensile strength, unit is megabeat ( MPa);
Maximum tensile force, in Newton (N);
Width of the middle part of the specimen, in millimeters (mm); -- Thickness of the specimen, in millimeters (mm). d
The elongation at break of the specimen is calculated according to formula (2), accurate to 1%: E 100(L - L)/L
where:
E|| tt||Elongation at break, the unit is percentage (%); the distance between the initial marking lines of a specimen is 25mm;
L
L, the distance between the marking lines is high when the specimen breaks, the unit is Meters (mm), calculate the arithmetic mean of five longitudinal or transverse specimens as the test results. 5.5.3 Tensile properties of L and W type coils
5.5.3.1 Test steps
GB12953—2003
Unit: mm
1
-(2)
The test piece is cut according to the requirements of Figure 1 and Table 4. The test piece is shown in Figure 3 and is in compliance with GB/T13022-1991. The tensile speed is (250±50) mm. /min, the clamp spacing is 50mm, place the test piece in the center of the holder and clamp it without twisting, and start the tensile testing machine. Read the maximum tensile force P of the specimen, and the length of the clamp when the specimen breaks, L
5.5.3.2 Result Calculation
The tensile force of the specimen is calculated according to formula (3), accurate to 1N/cm: T=P/E
Where:
T
P
B-
The tensile force of the specimen, the unit is Newton per meter (N/ cm); Maximum tensile force, unit is Newton (N):
Width of the middle part of the specimen, unit is cm (cm). -(3)
GB 12953—2003
A---total length 120;
B——parallel part width 10±0.5
length of gauge section 40±0.5;
—end width 25±0.5
D
R—large radius 25±2;
small radius 14±1
c | tt||In the formula:
E—elongation at break, unit is percentage (%): L:—the distance between the initial clamps of the specimen is 50mm; L,—the distance between the clamps when the specimen breaks, The unit is millimeter (mm), and the arithmetic mean of five longitudinal or transverse specimens is calculated as the test result. 5.6 Heat treatment dimensional change rate
5.6.1 Air blast oven
The control panel range is (room temperature ~ 200)℃, the temperature control accuracy ±2℃, 5.6.2 Test steps
Unit: mm | Reference lines for front and back. Under standard test conditions, press a steel ruler on the test piece, use a vernier caliper to measure the initial length S at the vertical and horizontal lines of the test piece, accurate to 0.1mm, and place the test piece flat on a glazed tile pad sprinkled with a small amount of talcum powder. On the board, place the backing board horizontally in a blast oven at (80 ± 2) C without being exposed, and keep it constant at this temperature for 24 hours. Take it out and place it under standard test conditions for 24 hours, and then measure the length S at the vertical and horizontal lines, accurate to 0.1mm.
5.6.3 Result Calculation
The longitudinal and transverse dimensional change rates are calculated separately according to Equation (5), accurate to 0.1%: RS,-S. 1 / S, mm): The length of a specimen after processing in the same direction as S, unit is 1 meter (mm). S,
Calculate the average of the longitudinal or transverse dimensional change rates of the three specimens as the longitudinal or transverse test results. (5)
2
Handle:
One upward plate,
One turn:
4 - Downward plate:
5 , 6 - Pitch-adjustable screw,
5.7 Low temperature bendability
5.7.1 Test equipment
120
128
Figure 4 bending instrument| |tt||5.7.1.1 Low temperature chamber: adjustment range (0~~-30)℃. Control accuracy ±2℃, GB12953-2003
Unit: mm
5.7.1.2 Bending instrument : The distance between the upper and lower plates made of metal can be adjusted arbitrarily, and the shape and size are shown in Figure 4. 5.7.2 Test steps bZxz.net
Cut the test piece according to Figure 1 and Table 4. With the water surface of the test piece facing outward, bend it 180° so that the 50mm wide edges overlap and are flush and fixed. Place the bending instrument Adjust the distance between the upper and lower plates to 3 times the thickness of the coil. GB12953-2003
Turn over the bending instrument and place the two specimens flat on the lower plate. The overlapping side faces the rotating axis and is 20mm away from the rotating axis. Put the bending instrument and the test piece into the low temperature box at the set temperature. After reaching the specified temperature, place it at this temperature for 1 hour. Then press the upper plate 1 internally at the temperature specified in the standard to reach the adjusted spacing position, and then take out the specimen after holding this position for 1 s. After returning to room temperature, observe whether the bend is broken, or use a 6x magnifying glass to observe whether there are cracks on the side bend of the specimen. 5.8 Resistance to perforation
Unit: mm
glass tube;
2
-dyed water,
3-filter paper:
4 -
Sample:
5 Glass plate:
6-—Sealant.
Figure 5 Perforation water tightness test device
5.8.1 Test instrument
5.8.1.1 Perforation meter: It consists of a metal conduit with a scale and a movable weight that can move freely in it. Hammer, locking bolt and hemispherical steel ball 8
1 blast oven
The control panel range is (room temperature ~ 200) ℃, the temperature control accuracy is ±2 ℃, 5.6.2 test steps
Unit: mm
(4)||tt ||Cut the test piece according to Table 4 in Figure 1. The size of the test piece is a square of 100mm × 100mm. Mark the vertical and horizontal directions. Draw a line at the measurement point on each side as a reference line before and after processing of the test piece. Under standard test conditions, press a steel ruler on the test piece, use a vernier caliper to measure the initial length S at the vertical and horizontal lines of the test piece, accurate to 0.1mm, and place the test piece flat on a glazed tile pad sprinkled with a small amount of talcum powder. On the board, place the backing board horizontally in a blast oven at (80 ± 2) C without being exposed, and keep it constant at this temperature for 24 hours. Take it out and place it under standard test conditions for 24 hours, and then measure the length S at the vertical and horizontal lines, accurate to 0.1mm.
5.6.3 Result Calculation
The longitudinal and transverse dimensional change rates are calculated separately according to Equation (5), accurate to 0.1%: RS,-S. 1 / S, mm): The length of a specimen after processing in the same direction as S, unit is 1 meter (mm). S,
Calculate the average of the longitudinal or transverse dimensional change rates of the three specimens as the longitudinal or transverse test results. (5)
2
Handle:
One upward plate,
One turn:
4 - Downward plate:
5 , 6 - Pitch-adjustable screw,
5.7 Low temperature bendability
5.7.1 Test equipment
120
128
Figure 4 bending instrument| |tt||5.7.1.1 Low temperature chamber: adjustment range (0~~-30)℃. Control accuracy ±2℃, GB12953-2003
Unit: mm
5.7.1.2 Bending instrument : The distance between the upper and lower plates made of metal can be adjusted arbitrarily, and the shape and size are shown in Figure 4. 5.7.2 Test steps
Cut the test piece according to Figure 1 and Table 4. With the water surface of the test piece facing outward, bend it 180° so that the 50mm wide edges overlap and are flush and fixed. Place the bending instrument Adjust the distance between the upper and lower plates to 3 times the thickness of the coil. GB12953-2003
Turn over the bending instrument and place the two specimens flat on the lower plate. The overlapping side faces the rotating axis and is 20mm away from the rotating axis. Put the bending instrument and the test piece into the low temperature box at the set temperature. After reaching the specified temperature, place it at this temperature for 1 hour. Then press the upper plate 1 internally at the temperature specified in the standard to reach the adjusted spacing position, and then take out the specimen after holding this position for 1 s. After returning to room temperature, observe whether the bend is broken, or use a 6x magnifying glass to observe whether there are cracks on the side bend of the specimen. 5.8 Resistance to perforation
Unit: mm
glass tube;
2
-dyed water,
3-filter paper:
4 -
Sample:
5 Glass plate:
6-—Sealant.
Figure 5 Perforation water tightness test device
5.8.1 Test instrument
5.8.1.1 Perforation meter: It consists of a metal conduit with a scale and a movable weight that can move freely in it. Hammer, locking bolt and hemispherical steel ball 8
1 blast oven
The control panel range is (room temperature ~ 200) ℃, the temperature control accuracy is ±2 ℃, 5.6.2 test steps
Unit: mm
(4)||tt ||Cut the test piece according to Table 4 in Figure 1. The size of the test piece is a square of 100mm × 100mm. Mark the vertical and horizontal directions. Draw a line at the measurement point on each side as a reference line before and after processing of the test piece. Under standard test conditions, press a steel ruler on the test piece, use a vernier caliper to measure the initial length S at the vertical and horizontal lines of the test piece, accurate to 0.1mm, and place the test piece flat on a glazed tile pad sprinkled with a small amount of talcum powder. On the board, place the backing board horizontally in a blast oven at (80 ± 2) C without being exposed, and keep it constant at this temperature for 24 hours. Take it out and place it under standard test conditions for 24 hours, and then measure the length S at the vertical and horizontal lines, accurate to 0.1mm.
5.6.3 Result Calculation
The longitudinal and transverse dimensional change rates are calculated separately according to Equation (5), accurate to 0.1%: RS,-S. 1 / S, mm): The length of a specimen after processing in the same direction as S, unit is 1 meter (mm). S,
Calculate the average of the longitudinal or transverse dimensional change rates of the three specimens as the longitudinal or transverse test results. (5)
2
Handle:
One upward plate,
One turn:
4 - Downward plate:
5 , 6 - Pitch-adjustable screw,
5.7 Low temperature bendability
5.7.1 Test equipment
120
128
Figure 4 bending instrument| |tt||5.7.1.1 Low temperature chamber: adjustment range (0~~-30)℃. Control accuracy ±2℃, GB12953-2003
Unit: mm
5.7.1.2 Bending instrument : The distance between the upper and lower plates made of metal can be adjusted arbitrarily, and the shape and size are shown in Figure 4. 5.7.2 Test steps
Cut the test piece according to Figure 1 and Table 4. With the water surface of the test piece facing outward, bend it 180° so that the 50mm wide edges overlap and are flush and fixed. Place the bending instrument Adjust the distance between the upper and lower plates to 3 times the thickness of the coil. GB12953-2003
Turn over the bending instrument and place the two specimens flat on the lower plate. The overlapping side faces the rotating axis and is 20mm away from the rotating axis. Put the bending instrument and the test piece into the low temperature box at the set temperature. After reaching the specified temperature, place it at this temperature for 1 hour. Then press the upper plate 1 down at the temperature specified in the standard to reach the adjusted spacing position, and then take out the specimen after holding this position for 1 s. After returning to room temperature, observe whether the bend is broken, or use a 6x magnifying glass to observe whether there are cracks on the side bend of the specimen. 5.8 Resistance to perforation
Unit: mm
glass tube;
2
-dyed water,
3-filter paper:
4 -
Sample:
5 Glass plate:
6-—Sealant.
Figure 5 Perforation water tightness test device
5.8.1 Test instrument
5.8.1.1 Perforation meter: It consists of a metal conduit with a scale and a movable weight that can move freely in it. Hammer, locking bolt and hemispherical steel ball 8
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