Chemical Industry Standard of the People's Republic of China HG/T2665—95 Reactive Yellow (Reactive Yellow 1995-04-05 Issued Ministry of Chemical Industry of the People's Republic of China K-4 G) 1996-01-01 Implementation WChemical Industry Standard of the People's Republic of China Reactive Yellow (Reactive Yellow Subject Content and Scope of Application K-4G) HG/T2665—95 This standard specifies the technical requirements, test methods, inspection rules and marking, packaging, transportation and storage of reactive yellow K-4G. This standard applies to reactive yellow K-4G, whose chemical structure belongs to monochloro-s-triazine type azo dye. 2 Reference standards GB2374 General conditions for dyeing determination GB/T2381 Determination of insoluble matter content in dyes GB/T2383 3 Determination of screening fineness of dyes GB/T2386bZxz.net GB/T2388 GB/T2390 GB/T2392 Determination of moisture content in dyes and dye intermediates Determination of color and intensity of reactive dyes Determination of pH value of reactive dyes Determination of thermal stability of reactive dyes 3 Test method for color fastness of reactive dyes GB/T2393 GB3920 GB3921 GB3922 GB6152 GB8427 Test method for color fastness of textiles to rubbing Test method for color fastness of textiles to washing Test method for color fastness of textiles to perspiration Test method for color fastness of textiles to hot pressing (ironing) Test method for color fastness of textiles to light (xenon arc) 3 Test method for color fastness of textiles to chlorinated swimming pool water GB8433 HG/T2—801 Determination of solubility of reactive dyes 3 Technical requirements 3.1 The formulations of Reaction Yellow K-4G are divided into powder, low dust powder and granules. 3.2 The appearance of Reaction Yellow K-4G is yellow uniform powder or granules. 3.3 The quality of Reaction Yellow K-4G shall meet the requirements of Table 1. Approved by the Ministry of Chemical Industry of the People's Republic of China on April 5, 1995 and implemented on January 1, 1996 W.(1) Strength, points (2) Color light (3) Water-insoluble matter content, % (4) Moisture content, % (5) Fineness (content of residue passing 180μm sieve), %(6) Solubility (50℃), g/L (7) pH value (8) Printing fixation rate, % (9) Thermal stability (strength reduction), points Note: Low dust and granular fineness are exempted from inspection. HG/T2665-95 3.4 The color fastness of the reactive yellow K-4G sample printed on cotton fabric shall not be lower than that specified in Table 2. Table 2 (Xenon arc) Note: Under the conditions specified in this standard, 1/1 printing depth is equivalent to 3% (owf). 4 Test method 4.1 Appearance Measured by visual method. 4.2 Determination of printing color and intensity 100% of the standard Similar to the standard~slightly 5 (basic color change) 200℃ Available chlorine 50mg/L Carry out in accordance with the provisions of GB/T2388. Printing depth is 3%, alkali agent sodium bicarbonate is 15g/L, steaming time is 7min, and gauge pressure is 0.5MPa. 4.3 Determination of water-insoluble content Carry out in accordance with the provisions of 1 in GB/T2381. 4.4 Determination of moisture content According to the provisions of 2 in GB/T2386. 4.5 Determination of sieving fineness of powdered dye According to the provisions of GB/T2383. 4.6 Determination of solubility According to the provisions of HG/T2-801. Wbzsoso,cO4.7 Determination of pH value According to the provisions of GB/T2390. 4.8 Determination of printing fixation rate According to the provisions of GB/T2393. 4.9 Determination of thermal stability According to the provisions of GB/T2392. 4.10 Determination of color fastness to printing 4.10.1 Determination of color fastness to light Perform in accordance with the provisions of GB8427. 4.10.2 Determination of color fastness to washing Perform in accordance with the provisions of Method 4 in GB3921. 4.10.3 Determination of color fastness to abrasion Perform in accordance with the provisions of GB3920. 4.10.4 Determination of color fastness to perspiration Perform in accordance with the provisions of GB3922. 4.10.5 Determination of color fastness to heat pressing (ironing) shall be carried out in accordance with the provisions of GB6152. 4.10.6 Determination of color fastness to chlorinated swimming pool water shall be carried out in accordance with the provisions of GB8433. 5 Inspection rules 5.1 Inspection classification HG/T2665—95 The inspection of Reaction Yellow K-4G is divided into factory inspection and type inspection. 5.1.1 Factory inspection Items (1) to (6) in 3.2 of this standard and Table 1 are factory inspection items. Thermal stability and printing fixation rate are generally inspected once every production cycle. If the continuous production lasts for more than one month, the inspection is carried out once a month. 5.1.2 Type inspection The technical indicators specified in Article 3.23.4 of this standard are type inspection items. If one of the six situations specified in Article 6.6.1 of GB1.3 occurs, type inspection should be carried out. In normal continuous production, inspection should be carried out once every six months. 5.2 Sampling method VN/2 barrels are selected from each batch of products (a batch is a uniform product mixed once) for sampling (N is the number of barrels of each batch of products). The number of small batch samples shall not be less than 3 barrels. When sampling, do not allow foreign impurities to fall into the product. Use a stainless steel sampling needle with the back facing up and insert it into the bottom of the barrel at an angle. Rotate the needle 180° and slowly pull it out to take out the sample. After fully mixing the sample, take a total of not less than 200g of the sample and put it into two clean, dry, ground-mouth brown wide-mouth bottles. Seal the bottle mouth with wax and label it with the manufacturer's name, product name, batch number, production date, etc. One bottle is submitted to the quality supervision department for inspection, and the other bottle is kept for future reference. 5.3 Factory Inspection Reaction Tender Yellow K-4G should be inspected by the quality supervision department of the manufacturer. The manufacturer should ensure that the quality of all reaction tender yellow K-4G shipped from the factory meets the requirements of this standard and is accompanied by a quality certificate in a certain format. 5.4 User Acceptance The user unit has the right to accept the reaction tender yellow K-4G received in accordance with the provisions of this standard. When the supply and demand parties have objections to the product quality, they can negotiate and resolve it. 5.5 Retest WHG/T2665—95 If one of the indicators in the test results does not meet the requirements of this standard, samples should be taken from the packaging barrels with twice the amount for retest. Even if only one indicator in the retest results does not meet the requirements of this standard, the entire batch of reaction tender yellow K-4G is unqualified. 5.6 Arbitration When arbitration is required, the arbitration unit can be selected by negotiation between the two parties. The arbitration method shall be in accordance with the provisions of this standard. 6 Marking, packaging, transportation, purchase and storage 6.1 The packaging barrels should have firm and clear markings, indicating the manufacturer's name, product name, registered trademark, production date, batch number, gross weight, net weight, and each batch of packaging should be accompanied by a product quality certificate, and the certificate should be marked with the number of this standard. 6.2 The finished product should be packaged in an iron barrel lined with a plastic bag. The plastic bag should be tied and then sealed with a lid. 6.3 It should be handled with care during transportation to prevent moisture and heat. 6.4 Finished products should be stacked on pillows and stored in a ventilated, dry place, away from high temperature and fire sources. They should not be stacked together with flammable materials. They should be kept clean and intact. The storage period is two years. Additional remarks: This standard is proposed by the Technical Supervision Department of the Ministry of Chemical Industry of the People's Republic of China. This standard is under the jurisdiction of the Shenyang Chemical Research Institute of the Ministry of Chemical Industry. This standard was drafted by Jiangsu Taixing Dyestuff Chemical General Factory. The main drafter of this standard is Li Yunsheng. W.bzsoso.cOm Tip: This standard content only shows part of the intercepted content of the complete standard. If you need the complete standard, please go to the top to download the complete standard document for free.