QB/T 1779-1993 Ethyl benzoate QB/T1779-1993 Standard download decompression password: www.bzxz.net

Industry Standard of the People's Republic of China
QB 1769~-1801—93
Fragrance Standard
(Product Standard)
Published on 1993-04-29
Implemented on 1993-12-01
Published by the Ministry of Light Industry of the People's Republic of China
Subject Content and Applicable Scope
Industry Standard of the People's Republic of China
Ethyl benzoate
This standard specifies the technical requirements, test methods and inspection specifications for ethyl benzoate. Applicable to the preparation of benzoic acid with benzoic acid and ethyl acetate by chemical reaction. Reference standards CB/T14454.3 Color test method GR/T1-454.2 Determination of external aroma odor GB/T14254.12 Determination of refractive index of spices GB/T14254.12 Determination of trace amounts of benzoic acid B4 Determination of the content of benzoic acid in whole or in part B/T14454.5 Determination of the content of benzoic acid in whole or in part B/T14454.6 Determination of the content of benzoic acid in whole or in part D/T14457 .1 Isolated and synthetic spices 2. Determination of the concentration of isolated and synthetic spices in GB68 or the general method for the analysis of spices by gas phase column filling 3 Product chemical name, molecular formula, structural formula, molecular weight Chemical name Chen Huawei Ai Yi Ester
Molecular formula C, HO.
Structural formula U, H, CUUCH, CH
Molar mass 1.18 (according to the original 188 National Music) 4 Technical requirements
Color Light color Transparent, color not exceeding standard liquid No. 4 4.2 Aroma Fruity, slightly oily,
Degree Density (25/25)
4.4 Refractive index (21 0>
4.5 Acid value 1, U.
1.5D-1.5o6c.
4.6 ().
4.7 Electrolysis 23)
4.8 Micro blood spots containing blood (with head)
Epidemic reaction
Ministry of Light Industry of the People's Republic of China: 993·04:·29 approved QB 177993
1883-1201 implementation
5 Test methods
5.1 Determination of color yield
JGR/T14454.2.
5.2 Evaluation of aroma
See GE/T14454.2
5.3 Determination of relative density, 25/2 yuan ℃
GB 1154n.
5.4 Determination of refractive index
IGE/T 144h4.:
5.5 Determination of acid value
See 68/T 14157...bzxZ.net
5.B Determination of sodium sulfide content
See CB/F 11437.0.
, proposed determination method see Appendix:
5.7 Determination of solubility
JGB/T 14457.1.
5.9 Determination of micromolarity
GB/T 4454.12,
6 Inspection rules
09 1779 -93
.1 Each batch of finished products should be accompanied by a production inspection certificate: "Production inspection" should ensure that all products meet the requirements of this standard. Each batch of products should be accompanied by a quality certificate, which includes the manufacturer's name, product name, trademark, date of manufacture, batch number, product certification and the number of this standard: 2 The acceptance unit has the right to accept the items of this standard and inspect the received products to see if they meet the requirements of this standard. One batch is inspected once, and different numbers are inspected separately. 6.3 For each batch of packaging units, two (bottles) are selected for analysis if the number is less than 1 (bottle) and three (bottles) are selected for analysis if the number is more than 1 (two). When opening the package for sampling, check the moisture and quality of the product on the outside, then vibrate to mix it, take the sample from the bottle (suck the sample evenly), inject it into the sampler, and put it into two bottles respectively. Note: manufacturer and product name, batch number, quantity and sampling date. Keep one bottle for inspection: see the inspection point for future reference. 6.4 If any of the following inspection results do not meet the requirements, The manufacturer may retake samples for re-testing. If the re-testing results still show unqualified indicators, the batch will not be accepted. .5 When the quality of the product is different between the supplier and the developer, the two parties may solve the problem or the legal inspection agency shall be responsible for the cost.
6.6 Color, gas, acid resistance, and chemical content are factory inspection indicators. Relative humidity, refractive index, irradiation, and micro-brightness are type inspection indicators: dynamic range is measured once. — 45 -
7 Marking, packaging, transportation, storage
Q8 177993
7.1 The formaldehyde should be packed in a fuel barrel or a fire extinguisher: the product name, manufacturer name, trademark, batch number, net weight, tare weight, factory date, standard code and relevant packaging special marks should be marked on the outside of the package. If there are special requirements in the order form, they can be negotiated with the manufacturer.
.2 During transportation, it should be prevented from being exposed to the sun, rain and foreign air pollution, and should be strictly protected from acid and water. 7.3 The product should be stored in a dry, ventilated, and shaded warehouse. Prevent foreign air pollution and keep away from fire sources. 7.4 Under the specified transportation conditions, packaging is complete, and the product is not opened, the warranty period is one year. 46
A1 instrument
281779—93
Agglomerate A
Testing room gas chromatography internal normalization method (toxicity tester)
A1.: Chromatography instrument, recorder and micro-processing emulsion according to the provisions of room 5 in GD11239,
A1-2 column
filling length ~, internal ~,
intercalation PEG0M, 6%~10% talked about Chrome
-4》wAw MCs an-8.day.1.
A1.3 detector
flame ionization detector
A2 dyeing case
color process temperature rise from 8u℃～2unC, relative humidity 3C/mi:
reasonable opening 218t.
detector 210℃
2,2 speed
gas flow trace atmosphere: 25nl/aim..
A3 column efficiency determination||tt| |A3.1 Chemical extraction test
The test shall be carried out in accordance with the provisions of Article 8.1 of GB119-1999, and the requirements shall be met.
A3.2 Silicone standard
The column efficiency shall be determined in accordance with Article 8.2 of CB119. A4 Test method
The internal normalization method shall be carried out in accordance with the standard method of Article 11.1 of GB153. A5 Repeatability and result expression
The test shall be carried out in accordance with the provisions of Article 11.1 of CB11530, and the requirements shall be met. Additional information:
Q8 1773-93
This standard is prepared by the Department of Measurement and Standardization of the Ministry of Light Industry
This standard is under the jurisdiction of the National Standardization Center. This standard is issued by Shanghai, responsible for the production of this standard. The standard is based on the standard of the Fruit and Oil Association of China 04N0.210. The original standard of the Ministry of Light Industry S05-3 is used for assembly. 45
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