HG/T 3004-1999 Light Fast Yellow 10G HG/T3004-1999 Standard download decompression password: www.bzxz.net

HG/T3004--1999bzxz.net
This standard is a revision of the chemical industry standard HG/T3004-1983 "Fast Yellow 10G". The technical content has been increased and some changes have been made.
The important technical differences between this standard and HG/T3004-1983 are as follows: 1. Adding four requirements for water resistance, acid resistance, alkali resistance and oil resistance; changing the names of the two items of color light and moisture to color and 105C volatile matter respectively; changing the color comparison from the original comparison with the standard sample to the comparison with the agreed sample; changing the relative tinting strength from the original comparison with the standard sample to the comparison with the agreed sample, changing the index from the original 95%~105% to not less than 100%, and changing the oil absorption range from the original 25%~~45% to (25~40) g/100g, both indicators have been improved; 1. The test methods of color light, tinting strength, moisture, water-soluble matter and oil absorption in 1983 are converted into the corresponding new national standards. This standard will replace HG/T3004-1983 from the date of implementation. This standard is proposed by the Technical Supervision Department of the former Ministry of Chemical Industry of the People's Republic of China. This standard is under the jurisdiction of the National Technical Committee for Standardization of Paints and Pigments. This standard was drafted by: Changzhou Paint Chemical Research Institute, Ministry of Chemical Industry. The main drafters of this standard are: Zheng Wenjuan, Jin Liandi. 912
1 Scope
Chemical Industry Standard of the People's Republic of China
Fast yellow 10G
Fast yellow 10G
This standard specifies the requirements, test methods, marking and packaging of fast yellow 10G. HG/T 3004—1999
Replaces HG/T3004:1983
This standard applies to yellow pigments produced by coupling reaction of o-nitro-p-chloroaniline with o-chloroacetoacetaniline after diazotization. The products are mainly used in inks, coating printing pastes and cultural and educational supplies. Structural formula:
Experimental formula: C1H20,N,Clz
CHCONH
Relative molecular mass: 395.30 (1991 International Relative Atomic Mass) 2 Referenced standards
The provisions contained in the following standards constitute the provisions of this standard through reference in this standard. When this standard is published, the versions shown are valid. All standards will be revised, and the parties using this standard should explore the possibility of using the latest versions of the following standards. GB1250--1989 Method for expressing and determining limit values ​​GB/T1710-1979 Method for determining light fastness of pigments GB/T 1715--1979
Method for determining the residue on sieves of pigments
GB/T1864--1989 Comparison of pigment colors (eqvISO787-1:1982) GB/T 5211. 2—1985
Determination of water-soluble matter in pigments by hot extraction method (negISO787-3:1979) Determination of volatile matter of pigments at 105℃ (eqvISO787-2:1981) GB/T 5211.3—1985
GB/T 5211.5—1985
Determination of water resistance of pigments
GB/T5211.6—1985Determination of acid resistance of pigments5Determination of alkali resistance of pigments
GB/T 5211. 7---1985
GB/T5211.8--1985Determination of oil resistance of pigmentsDetermination of oil absorption of pigments (eqvISO787-5:1980)GB/T 5211.15--1988
GB/T5211.19—1988Determination of relative tinting strength and dilution color of coloring pigments-Visual comparison method
(eqv ISO 787-16: 1986)
GB 9285-—1988
Sampling of raw materials for paints and varnishes (eqvISO842:1984) HG/T2457—1993 General rules for inspection, marking, packaging, transportation and storage of pigment products Approved by the State Bureau of Petroleum and Chemical Industry on April 20, 1999 Implementation on April 1, 2000
3 Requirements
The products should meet the requirements listed in Table 1.
Color (compared with agreed sample)
Relative tinting strength (compared with agreed sample), %
105 (volatile matter, % (mass fraction)
Water-soluble matter, % (mass fraction)
Oil absorption, g/100g
Sieve residue (400μm sieve hole), mass fraction, %Water resistance, grade
Acid resistance, grade
Alkali resistance, grade
Oil resistance grade
Light resistance, grade
Test method
HG/T 3004—1999
Requirements of Table 1
Approximately~micro
The product shall be sampled according to GB9285, and the sample shall be divided into two parts, one of which shall be sealed and stored for future reference, and the other shall be used as a test sample. 4.1 Color comparison
Perform according to the provisions of GB/T1864. The sample size is 0.5g, and the amount of refined linseed oil added for the first time is 1ml. After grinding for 200 turns, add 0.8mL and grind for another 25 turns.
4.2 Determination of relative tinting strength
Perform according to the provisions of GB/T5211.19. The grinding concentration of the pigment dispersion adopts 1.0g pigment. material and 1.5g paint base, the grinding speed of the pigment dispersion is 200 turns, the dilution ratio is 1:10, that is, 0.30g of colored pigment paste and 3.0g of white pigment paste. 4.3 Determination of 105C volatile matter
According to the provisions of GB/T5211.3. The sample size is 5g. 4.4 Determination of water-soluble matter
According to the provisions of GB/T5211.2. The sample size is 2.5g. 4.5 Determination of oil absorption
According to the provisions of GB/T5211.15. The sample size is 2g. 4.6 Determination of sieve residue
According to the provisions of GB/T1715-1979 3. 4.7 Determination of water resistance
shall be carried out in accordance with the provisions of GB/T5211.5-1985. The preparation of the test solution shall be in accordance with the provisions of 3.1.1: 4.8 Determination of acid resistance
shall be carried out in accordance with the provisions of GB/T5211.6. The result is expressed as the color of the filtrate. 4.9 Determination of alkali resistance
shall be carried out in accordance with the provisions of GB/T5211.7. The result is expressed as the color of the filtrate. 4.10 Determination of oil resistance
shall be carried out in accordance with the provisions of GB/T5211.8.
4.11 Determination of light resistance
shall be carried out in accordance with the provisions of GB/T1710 The light fastness test is carried out using the light fastness machine method. All the technical requirements listed in this standard are type inspection items, among which color, relative tinting strength, volatile matter at 105℃, water-soluble matter, 9
HG/T3004
oil absorption, and sieve residue are factory inspection items. Under normal production conditions, type inspection shall be carried out at least once a year. The judgment of the inspection results in this standard shall be carried out in accordance with the provisions of 5.2 of GB1250-1989. 5 Marking and packaging
5.1 Marking
shall be carried out in accordance with the provisions of Chapter 4 of HG/T2457-1993, and a quality certification mark shall be added. 5.2 Packaging
shall be carried out in accordance with the provisions of Chapter 5 of HG/T2457-1993. Products can be made of iron barrels, wooden barrels, cardboard barrels, fiberboard barrels or fiber woven bags lined with plastic film bags according to needs. 943
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