This standard specifies the technical requirements, test methods, inspection rules, marking, packaging, transportation, storage and safety precautions for industrial cresol. This standard applies to industrial cresol obtained by fractionation of crude phenol obtained from coal tar and phenol-containing wastewater. GB/T 2599-1997 Industrial cresol GB/T2599-1997 Standard download decompression password: www.bzxz.net
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GB/T 2599--1997 This standard is revised on the basis of GB2599-81 "Tri-Mixed Cresols". The name of the standard was changed from "Tri-Mixed Cresols" to "Industrial Cresols"; the standard content has been expanded to include scope, reference standards, marking packaging, transportation, storage and safety precautions; the technical content has been appropriately adjusted, and the first-grade product index of distillation test and moisture content has been cancelled; the second-grade product index of neutral oil content has been cancelled; and the moisture index has been revised to 1.0%. This standard will replace GB2599-81 from the date of its entry into force. This standard was proposed by the Ministry of Metallurgical Industry. This standard is under the jurisdiction of the Information Standards Institute of the Ministry of Metallurgical Industry. The drafting units of this standard are: Shanghai Meishan (Group) Co., Ltd. and the Information Standards Institute of the Ministry of Metallurgical Industry. The main drafters of this standard are: Zhang Yi and Sun Wei. This standard was first issued in 1981. 1 Scope National Standard of the People's Republic of China Technical cresol GB/T 2599—1997 Replaces GB2599—81 This standard specifies the technical requirements, test methods, inspection rules, marking, packaging, transportation, storage and safety precautions for industrial cresol. This standard applies to industrial cresol obtained by fractionation of crude phenol prepared from coal tar and phenol-containing wastewater. 2 Referenced standards The provisions contained in the following standards constitute the provisions of this standard through reference in the standard. At the time of publication of the standard, the versions shown are valid. All standards are subject to revision, and parties using this standard should explore the possibility of using the latest version of the following standards. GB 1999--80 Sampling method for light oil from coking products GB 2281-80 GB 2282-80 GB 2288—80 GB 2601--81 GB 2602—81 GB 3711—83 GB 5074—85 GB 8170—87 3 Technical requirements Determination method of density of phenolic products Distillation test method of phenolic products Determination method of moisture content of coking products Gas chromatography determination method of composition of phenolic productsUrea determination method of meso-cresol content of phenolic productsDetermination method of neutral oil and pyridine base content of phenolic productsMicrocoulometric determination method of moisture content of coking productsNumerical rounding rules The technical indicators of industrial cresols shall comply with the provisions of Table 1: Table 1 Indicator name Density (20℃), g/cm2 Distillation test (atmospheric pressure 1 01325Pa)Distillate before 190℃ (V/V), % Distillate before 210℃ (V/V), %wwW.bzxz.Net Meta-cresol content, % Neutral oil content, % Water content, % Approved by the State Bureau of Technical Supervision on March 17, 1997Not more than Not less than Not less than Not more than Not more than Colorless to brownish red transparent liquid 1.03~1.05 Implemented on September 1, 1997 4 Test method GB/T 2599—1997 4.1 Determination of appearance: Pour the sample into a colorless transparent glass test tube with an inner diameter of 22mm and observe its color visually under transmitted light. 4.2 The density shall be determined in accordance with GB2281. 4.3 The distillation test shall be carried out in accordance with GB2282. 4.4 The content of m-cresol shall be determined in accordance with GB2601 or GB2602; GB2602 shall be used for arbitration. 4.5 The content of neutral oil shall be determined in accordance with GB3711. 4.6 The content of water shall be determined in accordance with GB2288 or GB5074; GB2288 shall be used for arbitration. 5 Inspection rules 5.1 The quality inspection and acceptance of industrial cresol shall be the responsibility of the quality supervision department. 5.2 The sampling and preparation of samples shall be carried out in accordance with GB1999. 5.3 The test values shall be rounded off in accordance with GB8170. 6 Marking, packaging, transportation and storage 6.1 The product shall be packed in clean and dry iron barrels or tank trucks, and the barrels shall be marked with the product name, manufacturer name, net weight, grade and "toxic" mark. 6.2 Each batch of products leaving the factory should be accompanied by a quality certificate, which should include: manufacturer name, product name, standard number, batch number, gross weight, net weight, delivery date and various test results and quality grades specified in this standard. 6.3 Keep away from fire and heat sources during transportation and storage, and pay attention to ventilation. It should be stored separately from oxidants. If stored in the open air, prevent rain from seeping in. 7 Safety precautions 7.1 Cresol is an organic corrosive. It is flammable, corrosive and toxic. The maximum allowable concentration in the workplace is 22mg/m2.7.2 Exhaust equipment should be installed in the workplace; necessary fire-fighting facilities and first aid kits should be prepared; personal protective equipment (such as protective glasses, rubber gloves, protective masks, masks, work clothes, etc.) must be used when entering the workplace. 7.3 If this product catches fire, it can be extinguished with mist water, foam, sand and soil. 7.4 If this product touches the skin, it should be washed off quickly with soapy water. 156 Tip: This standard content only shows part of the intercepted content of the complete standard. If you need the complete standard, please go to the top to download the complete standard document for free.