title>GB 4374.7-1984 Chemical analysis methods for magnesium powder and aluminum-magnesium alloy powders - Gravimetric method for determination of hydrochloric acid insoluble matter - GB 4374.7-1984 - Chinese standardNet - bzxz.net
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GB 4374.7-1984 Chemical analysis methods for magnesium powder and aluminum-magnesium alloy powders - Gravimetric method for determination of hydrochloric acid insoluble matter
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Standard ID:
GB 4374.7-1984
Standard Name: Chemical analysis methods for magnesium powder and aluminum-magnesium alloy powders - Gravimetric method for determination of hydrochloric acid insoluble matter
GB 4374.7-1984 Chemical analysis methods for magnesium powder and aluminum-magnesium alloy powders Gravimetric determination of hydrochloric acid insoluble matter GB4374.7-1984 standard download decompression password: www.bzxz.net
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中华人民共和国国家标准 镁粉和铝镁合金粉化学分析方法重量法测定盐酸不溶物量 Methods for chemical analysis of magnesium powdersand aluminium -magnesium alloy powdersThe gravimetric method for the determinationof insoluble content in hydrochloric acid本标准适用1镁粉中盐酸不溶物量的测定。测定范固:不人于0.20%。本标准遵宇GB1467-78《治金产品化学分析方法标准的总则及般规定》,方法提要bZxz.net UDC 669.721 + 669 715'721-492 GB 4374.7-84 试样用盐酸溶解后,过滤并灼烧残渣,根据盐酸不溶物质量计算其百分含量。试剂 2.1盐酸(1+1)。 2.2硝酸银溶液(1%)。 高温炉。 分析步骤 4.1测定数量 行测两份试样,取其均值 4.2试样量 称取5.00g试样。 4.3测定 4.3.1将试样(4.2)置于500ml烧杯中,用少量水润湖。4.3.2缓慢加人90ml盐酸(2.1),待试样完全溶解后点沸1min,取下,用定滤纸过滤,并用热水洗涤至滤出液用硝酸银溶液(2.2)检查无氨离了反应为出。4.3.3将滤纸及語酸不溶物(4.3.2置于己灼烧并称至恒肚的瓷址蜗中,先1炉灰化,然后催高温炉」700C灼烧40min,取壮,置于「燥器中,冷即全室温,称最,并重复灼烧全恒最。5 分析结果的计算 按下武让算喆酸不溶物的百分舍鼠:盐酸不溶物(%) 式中:m,--增埚利盐酸不溶物的质量,g;国家标准局19840430发布 19850401实施 充许差 性蜗的质最,; 试样最,g。 GB4374.7-84 实验室之间分析结果的差值应不大下表所列允许差。战酸不溶物鼠 .0.050 -.05 ~ 1.10 0.10~0.20 附加说明: 本标准由中华人民共利用金工业部提出,本标准的东北轻合金加!负资起草本标准山东北轻合金加广、西北加广起草。本标准主要起草人尤贵法、“亚车。162 充许差 -HTi KAoNi KAca- Tip: This standard content only shows part of the intercepted content of the complete standard. If you need the complete standard, please go to the top to download the complete standard document for free.