HG/T 3570-2001 Photographic chemicals Potassium bromide (for emulsion)
Some standard content:
I8 37.040.20:71, 040. 50
Chemical Industry Standard of the People's Republic of China
HIG/T356935702001
Determination of light absorption of color formers
Photographic chemicals Potassium bromide (for emulsion)
Published on January 24, 2002
Implemented on July 1, 2002
Published by the National Economic and Trade Commission
ICS 37.040.30
Customer number: 10130-2002
HIG/T3570-2001
This standard is a recommended chemical industry standard HG/T 257·198S clothing buckle grade wave chemical Xuan (milk 3 whole hit and reduced. This standard will be implemented from the month, the same as the generation of H: T70-1939. This standard is not issued by the State Administration of Petroleum and Chemical Industry Policy and Law. Six standards and ten national optical material standardization technical staff The main standard originator is Beijing Institute of Chemical Engineering. The originator of the standard is Li Huichi. This standard was first issued in 1988 as a professional standard 2G8500188.1695 and was adjusted to the standard of the chemical industry: Product No. HG/5-X
Chemical Industry Standard of the People's Republic of China
Photographic Chemicals
Potassium Aluminate (for emulsion)
Phnfingraphic rade chemlcalsPotasginm bromide fur emulsiun Formula: KBr
Relative molecular weight, 119. According to the original sample of the country in 1997) 1 Scope
HG/T 3570-2001
Replacement HGT357c-15KK
This standard specifies the technical requirements for the chemical evaluation of potassium alkylate emulsions: the test method, inspection rules, packaging, marking, storage in a machine. The main standard is applicable to the chemical evaluation of emulsions used in the preparation of oral emulsions: 2 Referenced standards
The texts contained in the following standards constitute the text of this standard by being referenced in this standard. When this standard is issued, the versions shown are all valid. All standards may be slightly revised, and the parties using this standard should use the following standard for the possibility of the latest version. Chemical test
GH/T 601-1988
GB/T 602
GH:T 603—1988
GB/T 619 -1383
GPT6682
GB/T$723
Chemical trial production
Chemical test
Isolation analysis (discarded analysis) Preparation of standard solvents for determination of impurities (n415 () 633-1332) Preparation of effective preparations used in the test method (ne1506353 [: 1082) Beijing Academic Standards
Sampling and acceptance standards
Analytical laboratory water specifications and test methods [cUV1S) 3196: 19H?) 1388
GH/T 1C721—198U
HG/T 3484—1999
3 Properties
Beijing Experimental College
General rules for flame atomic absorption spectrometry (negS()63531:2982), especially for roasted (graphite) raw materials, instantaneous absorption spectroscopy, chemical reagents
Standard for color change emulsion and clarity standard
This product is a concave color clear powder, which dissolves in water. 4 grid
Australia chemical containing KBr
water zeyi reaction
National Economic Committee 2002-01-21 approved version
2002-07-01 buy implementation
bright slip test road
According to agricultural bath pad.
heat chemical: C1). No.bzxZ.net
excited plate number R
settlement chemical will,
according to non
5 ice test
IIG/T35702001
table (）
Xi Xiang·Group
tsu.000cs
su.uuu c?
according to the first level
.0.003
u, Uuu 1
X3 0:
Except for the established ones, the standard titration solutions, standard starting liquid preparations and finished products in this inspection are all made from hot-drying materials of GT/T601 Ti02GT/T3, and the laboratory water used is in accordance with the third grade specification of 3/TGH2. The test pressing is refined to C.9 and weighed. 5.1 Weigh 0.4% or 0.6% potassium chloride in 1cc ml of water, add 5% ethyl acetate and 5g/mL sodium chloride, and titrate in a cup [c(AgVC) = u, ml/L protected from light until a milky white color appears. The total amount of potassium chloride is calculated as follows: Where: x is the mass fraction of potassium chloride, mX10Q0 is the volume of the effective titration with silver iodide standard, m1/mL is the volume of the effective titration with silver iodide standard, m1/mL is the volume of the effective titration with silver iodide standard, m2/mL is the concentration of the diluted solution, m3/mL is the mass fraction of the solution, and the titration rate is 11rm1 The content of carbon dioxide in the sample is not less than 1.5-1.5 when measured by a chromatometer. 5.3 Determination of turbidity test Weigh 20 test pieces and collect 100 L of water. The turbidity shall not exceed 440 °C. Photograph the secondary sample. 5.4 Determination of turbidity of water: In the water sample, keep it warm for 1 h and pass it through a constant weight pot. Wash the solution by heat to remove the ions. The filtration mass calibrator is as follows: 5.5 Mixed salt HG/T3570-2001 Weigh 2 test pieces and dissolve them in 21 μl. In water, / concentration of 1 L & 5r: L acid flow micro-[1/2H, SO, 11mol / L =. Change alliance 30mia. Jince new single yellow will not be compared with the standard liquid, the machine Ya batch of the melt to the sensitive acid standard liquid: intense phase first
5.6 oxide
. 02 mg Br01:
take 1 B sample, stomach shape, period 2F must nitric acid liquid 10C m1, on the water tank, if the heat will penetrate the color, wash the bottle wall with a small amount of water, continue to heat 1r:in cold indicator, 1U,mL silver acid standard full set drop laser c (AgXO, =U.1mal/=, add = titration H related pregnancy excess: m:nM30T. Ammonium ferric indicator 1ml with hydrochloric acid standard titration solution (VH, CNS).l/. New determination of melting chain and red driving, sulfur chain standard determination liquid tablets do not exceed: salt grade
vortex and secondary
5.7 specialization Weigh 1 sample, add 0.2mL of 10g/L freshly prepared nitrite solution (1/2HS () = 1.1ol/L) into 20ml bath. Take with 1m3 of trifluoromethane, and the red color should not be darker than that of standard comparison solution. Preparation of standard comparison solution contains the following: Iodide standard tape: Photographic grade 1
Secondary
Treat at the same time as the sample.
5.8 Phosphate
.n. 3s mg T:
Weigh 1 sample into 10ml water, 9% ethanol solution, 1ml of 10% saline. Add 1250g/L fluoride solution under constant shaking. Sieve 25ml. Heat. Let stand for 3min and the resulting solution will be dried to obtain a large amount of standard comparison solution. The preparation of the standard comparison wave is a slightly acidic monitoring wave containing the following data, photographed and scanned at the same time as the sample, and carried out in accordance with the provisions of G/T72. 5.9.1 Instrument conditions: light mud, hollow lamp. 348.81: flame: air-block.
5.9.2 Determination of the substance
0.42 ng 50
3.05mgs3,
Take 62.55g of the sample: add water to a 250ml volume, adjust the volume to the mark, add 10ml of the sample to each 125ml separatory funnel, add 2.4g, 6.1g of the standard solution, and then add 10/L of pyrrolidine-methylformic acid (AFTXC) solution to each separatory funnel: mT., adjust the pH to F with 1% acetaldehyde solution, and then accurately add ml of methyl isocyanate (MIK) to fill the lid to 2ain.Stand for 2 minutes, collect the organic phase, add 3.1mL MIBK to the water mixture for the second extraction. Combine the slices and extract the liquid twice, mix and then follow the determination of heat in 3.2.2 of GB/T9Y23-1588. 5.10 Weakness and lead cobalt
shall be determined according to the current determination of GB/T10721.
5.10. Apparatus and components
Light source: hollow cathode lamp;
Length: 344.7nml
Protective gas: hydrogen,
Light source: hollow cathode lamp:
Liquid length, 283.3mm
Protective gas: gold
Light source: hollow cathode lamp:
Wavelength: 222.9uml
Protective gas: sodium argon,
5.10.2 Determination method
5.10.2.1 Preparation of standard curve
[IC/T3570—2001
Take four 125L aliquots of juice, add 30 ml of water to each, add 1% water ... rg.0.2 μg.0.3Pg::0PP,0.15μK.0.25g,0,=R
:0. 0 μg,0. 25 ng,0. 5 wx,G. 75 ng. Add 10 g/L pyrrolidine-1-aldehyde (A1DKC>5 mL) to each separation funnel. Add 1% acetic acid to adjust the pH value to 5, then add 4 mL of isobutylbenzene (MEBK), plug the lid, add 1 mL of MEBK for 2 min, and let stand for 2 min. After separation, collect the organic phase: add 1 mL of MEBK to the aqueous phase for the second extraction. Combine the two extractions and determine according to G/T1072419496.2. 5.10.2.2 Determination of the selected extractions: Weigh 125 mL of sample, add water to a volume of 0.5 mL, and freshly dilute the extract. Add 10 mL of water to each of the four 125 mL separation funnels, accurately add 20 μL of the sample solution, one portion as the final sample, and the other three portions as standard 1.( , chain 0.5J + and then make the complexation according to the steps of making the standard curve. The organic rate is determined according to the provisions of 6.2.1 in G/T10721--1589. The lead content of the test sample is one or two times higher than that of the oxygen, so the amount of standard liquid added is also large. The staggered time should be reduced as much as possible. MIBK should be diluted 1I times.
5.11 The period can be negotiated with the user.
6 Rules
According to the provisions of GB/619 for sampling and acceptance, 7 Packaging, marking, transportation and storage
7.1 Packaging: Packaging units recommend more than 30 The inner package is a double-layer chain bag. The fiberboard barrel is used for packaging. Each barrel should have a special seal for production, such as a seal.
7.2 The inner package should be marked with the specified standard, product name, production date, batch number, and "same grade (for emulsion)". The inner package should have a quality certificate, including the manufacturer's name, product name, batch number, production date, net weight and energy (sensitivity test results) and standard number of the wood product that meets the requirements of this standard. 7.3 Transportation: Transportation should be carried out with caution and avoid heat and moisture. 7.4 Storage: Store in a dry, cool, and dry place.
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