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Thermal spraying—Powders—Composition and technical supply conditions

Basic Information

Standard ID: GB/T 19356-2003

Standard Name:Thermal spraying—Powders—Composition and technical supply conditions

Chinese Name: 热喷涂-粉末-成份和供货技术条件

Standard category:National Standard (GB)

state:in force

Date of Release2003-10-29

Date of Implementation:2004-05-01

standard classification number

Standard ICS number:Mechanical manufacturing>>Surface treatment and coating>>25.220.20 Surface treatment

Standard Classification Number:Comprehensive>>Basic Standards>>A29 Material Protection

associated standards

alternative situation:GB/T 12608-1990

Procurement status:ISO 14232:2000,MOD

Publication information

publishing house:China Standards Press

ISBN:155066.1-20463

Publication date:2004-03-01

other information

Release date:2003-10-29

Review date:2004-10-14

drafter:Cao Qing, Kuang Yizhuang, Wang Chunhua

Drafting unit:Wuhan Institute of Materials Protection

Focal point unit:National Technical Committee for Standardization of Metallic and Non-metallic Coverings

Proposing unit:China Machinery Industry Federation

Publishing department:General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China

competent authority:China Machinery Industry Federation

Introduction to standards:

This standard specifies the chemical composition and physical properties of powders commonly used in the production of thermal spray coatings. GB/T 19356-2003 Thermal spraying - Powders - Technical conditions for composition and supply GB/T19356-2003 Standard download decompression password: www.bzxz.net
This standard specifies the chemical composition and physical properties of powders commonly used in the production of thermal spray coatings.


Some standard content:

GB/T19356—2003
This standard adopts ISO14232:2000\Composition and technical conditions for supply of thermal spray powders” (English version). This standard redrafts ISO14232. According to the basic situation of thermal spray powder technology in my country, this standard makes the following modifications to ISO14232:
…——Cancel the prefix and prefix of the international standard:——Use “this standard” instead of “this international standard”——Quote the Chinese standard of the equivalent international standard: The latest version of ISO3310-1 is ISO3310-1:2000. Since my country has not yet converted it into a national standard, this standard still quotes this international standard.
GB/T1479.1—1984 covers the Scott volumetric method + GB/T1479.11984 replaces IS03923-2:1981 which specifies the Scott volumetric method and is used in this standard. This standard replaces GB/T12608—1990 "Method for naming materials for thermal spray coatings". This standard is proposed by the China Machinery Industry Federation and is under the jurisdiction of the National Technical Committee for Standardization of Metallic and Non-metallic Coatings. The drafting units of this standard are: Wuhan Institute of Material Protection, Weishen Thermal Spraying Material Research Institute, Chengdu Zhenxing Jinjie Powder Factory. The main drafters of this standard are: Cao Qing, Kuang Yimu, Gan Chunhua, Wu Zijian, Yan. 1
1 Scope
Thermal Spraying
Powder Composition and Technical Supply Conditions
This standard specifies the chemical composition and physical properties of powders commonly used in the production of thermal spray coatings. 2 Normative references
GB/T 193562003
The clauses in the following documents become the clauses of this standard through reference in this standard. For all referenced documents with dates, all subsequent amendments (excluding errata) or revisions are not applicable to this standard. However, parties that reach an agreement based on this standard are encouraged to study whether the latest versions of these documents can be used. For all undated referenced documents, the latest versions are applicable to this standard. GR/T1479 Determination of loose density of metal powders Part 1: Funnel method (neg1SD3923-2) GB/T1482 Determination of fluidity of metal powders Standard funnel method (Hall flowmeter) (nISO4490) GB/T5314--1985 Sampling method for powders for powder metallurgy (neqISO3954:) ISO3310-1:-1 Requirements and tests for test sieves Part 1: Wire cloth sieves 3 Properties of thermal spraying powders and their determination
3.1 Samples and sampling
Samples and sampling should be mixtures of uniform particle size. The corresponding sampling and sampling operation methods and equipment guidelines should comply with GB/T5314.
3.2 Chemical composition
The chemical composition can be determined by any appropriate test method, such as atomic absorption spectroscopy, flame emission spectroscopy, X-ray fluorescence analysis, chemical analysis, etc.
3.3 Particle size range
The typical particle size range applies to thermal spray powder feeding devices. When the particle size distribution is determined by the particle size measurement method in accordance with IS03310-1, the variation range of fine screening shall not exceed 2% and the variation range of coarse screening shall not exceed 5%. The apparent particle size depends on the measurement base technology, so the maximum permissible tolerance of the upper and lower particle size limits also depends on the measurement method. The measurement method, particle size range, and the maximum permissible tolerance of the upper and lower particle size limits should be agreed upon by the powder manufacturer and the thermal spray coating manufacturer to ensure the reproducibility of the thermal spray process.
The supplied powder should be suitable for thermal spraying process. The typical particle size range (in μm) available for thermal spraying process is as follows: -22/5;
-90/45
-45/5;
-63/16;
3.4 ​​Particle size distribution
In order to accurately express the particle size range, the particle size and its distribution must be measured. X-ray absorption method and laser beam scattering method are preferred because their reproducibility, rapidity and resolution are higher than traditional screening methods. The results of the determination of particle size and particle size distribution depend on the method used, and the powder is also affected by the solubility of the binder. Therefore, it must be published (150 3310-1: Revision of 1990). 1
GB/T 193562003
It is necessary to prove that the powder to be tested is suitable for the selected method. In addition to stating the results of the particle size distribution determination, the powder test certificate shall also state the test method used.
3.5 Manufacturing process - particle morphology
The powder production process shall be indicated, such as melting method, bonding method, agglomeration method, atomization method, etc. Scanning electron microscope and surface microscope can be used to show the particle shape and surface morphology, and the image can be compared with the sample provided by the manufacturer to determine the degree of similarity. Examples of the relationship between manufacturing process and particle morphology are shown in Appendix A. 3.6 Bulk density
The bulk density of the powder shall be determined in accordance with the provisions of GB/T1479 and expressed in g/cm2. 3.7 Flowability
The flowability of the powder shall be determined in accordance with the provisions of GB/T1482 and expressed in /50. 3.8 Microstructure
The microstructure can be determined by preparing metallographic specimens of cross-sections of the powder particles. Since the sample preparation method is critical, it should be agreed upon by the manufacturer and the user.
3.9 Determination of Phases
The type, amount, shape, structure, composition and size of the phases in multiphase powders can be determined by X-ray diffraction analysis, microprobe or metallography and quantitative image analysis.
3.10 Summary
The relative importance of various properties of thermal spray powders for different thermal spray processes and materials is shown in Table 1. Relative importance of various properties of thermal spray powders in various thermal spray processes and materials Chemical composition Pure metals Metal alloys Carbides, magnetites Metals, carbides Oxides, salts and other non-carbides Ceramics Organic materials Plasma spraying Melt spraying High speed flame spraying Particle shape Bulk density Powder types Different thermal spray processes Note: +1 indicates that the property is mandatory/strictly required. - indicates that the property is recommended/important. +1 indicates that the property is mandatory/strictly required. +1 indicates that the property is recommended/important. +1 indicates that the property is mandatory/strictly required. +1 indicates that the property is recommended/important. +1 indicates that the property is mandatory/strictly required. +1 indicates that the property is recommended/important. +1 indicates that the property is mandatory/strictly required. +1 indicates that the property is mandatory/important ...
Flowability
! Microstructure
In the spraying of organic materials, the oxidation resistance, thermal decomposition and capsule properties of the molten material are important. For spraying carbides and oxides, detailed regulations must be observed, such as Zr (, -Y, 0g, 2
phase separation! Melting range
Powder classification
4.1 General
Thermal spray powders can be classified according to chemical composition and can be divided into the following types: pure metal (4.2 and Table 2);
b) metal alloys and composite materials (4.3 and Tables 3 to 11) GB/T 19356-2003
carbides, carbides with metals, carbides with metal alloys, carbides with composite materials (4.4 and Table 12); c
oxides, phosphates and other non-carbide ceramics (4.5 and Table 13) d
organic materials (4.6).
Powders mixed with several components are not included. Pure metal
Table 2 Pure gold without powder
Main components
Metal alloys and metal composite materials
Abbreviation code
NiGuBSi76 20
NEBSi g6i
NiBSi 94
NiBSi95
NiCrBSi90 4
NiC-BSi865
NiCrBi885
0, 1~-0. 2
0. 1---0. 2
.0. 15
Chemical composition/(%)
Table 3 Self-fluxing metal alloy material powder
Chemical skin content/(%)
0.15~0.28Residue
0.15~-0.251Residue
NiC-BSiB310
0.15~0.253
NiCrESi858
NiCrBSi848
19~-20
1.8--2.0≤0. 5
11. 0 --1. 5
1. 5~2. 02. 8~3. 7
1.2~1.7:2.2~2,8
3.0~3.50.8~
1, 0--2. 01. 0-bzxZ.net
1. 5 ~- 3. 52. 0
812,8~3.5
1.0.≤0.5
GB/T 19356—2003
Abbreviation number
NiCreSi88 4
NiCrBSi80 11
2, 14
NiCrwRSi
64 11 16
NiCrCuMoB
St 67 17 3 3
0. 3--0. 4||tt| |0. 35~0. 6; margin
0.5~0.6 1 remainder
0. 5---(1. 7
NiCrCuMoWESi
i 0. 4--0. 6
6417333
2. 16) NiCrBSi 74 15
2. 17 NiCrBSi 65 25
. 18 NiCrBSi 74 14
NiCrBSi827||tt| |NiBSi92
2. 21, NiCoBSi 7120
CnCrNiMoBSi
40 18 27 5
CaC+NiMoRSi
50 18 17 6
CoCrNiwBSi
53 20 137
CoCrNiwBSi
52 19 15 9
CoCrNiWBSi
47 19 15 13
CoCrNiwBSi
45 19. 15 15
Box code
NiCr 80 20|| tt||0. 75--1. 1
0. 8-- 1. 4
0, 75~-1. 0
0. 8~ 1. 1| |tt||1. 0~1. 3
1. 3~-]. 6
16--17
19-~20
19--20
Table 3 (continued)
Chemical composition/《%》| |tt||15.5~16.5
[12. 5 ~~ 13. 5
14. 5~15, 5
Ni-Cr-Fe gold alloy material powder||tt ||Chemical Sense Method)
Residue 18~21
3. 2NiCrFe 75 15 8Residue 14--17Residue 17~20
3.3NiCrA174195||tt ||Margin|20 ~ 220.3 ~ 0.5
3.4 NiCrNb 70 21 4
Nic-Maw
54 16 17 5
NiCrAlMoFe
73 9 7 6
Remainder 1141 days
Margin 8~10
4 -~ 6
i16--18
1. 6-~2, 03, 0-~3, 5
2. 5-~3. 52. 0 ~2, 53. 5~4, 0Others
3. 5 ~4. 012. 3~~2. 7 3. 0~~3. 5]0.5|| tt||2. 5~3. 53.4~4.04.0~4.50. 5
3. 0~-5. 03. 5~~4. 0
4. 0-~4,5
3, 5~5.02. 8~ 3.5|| tt||4.0~4.5:
4. 0~5.02.75~3. 5
2. 5~3. 5
2. 75 ~ 3. d||tt ||4. 5~-4. 7
4. 0-~5. 0
3. 0. ~ 3. 43. D~3. 5
1. 5 -1. 82. 4-- 2, 5
1. 5-~1. 8;2. 4~ 2. 5
1. 5--2. 0|2. 0-2. 5
p. 40. 6p. 40. 6o. 30. 5
Input and writing guide| |tt||NiCriAl
75 20 3 2
NiCrCaAITi
6716944
NiCoCrAIMoTi
631510534
NiCoCtAJMoTi
57 17 11 5 6 4
NiCr50 50
NiCrMoNh
64 22 9 3. 5
NiCrCoM,TiAW
57 18 12 6 3 2 1
NiCINbFeA]
66 14 7 8 5 5
NiCrFeAIMo
68 14 7 5 5
NiCrAIMoTiC
68 8 7 5 2. 5
FeCrMgAl
6523 55
Margin 1B~ 221. 5 -- 2. 5
Remainder 15~17
Remainder 1012
Remainder 50~52
Remainder 20~23
Remainder 17~191.5~ 2.5
Set quantity 12--15
Remainder 7~10
Table 4 (continued)
Chemical composition/(%)
1~ 3 0_ 4~0.
14~16 2--4
15-1857
1~-13 5~~7
1SD14232:2000(E) has a content of zero, which is 11-13. We hereby correct it. The content of this item in ISO)14232:2000(F) is 11~13. It should be Etc., hereby corrected. Si
Table 5MCrAIY Gold Wing alloy material powder
Abbreviation code
NiCrAlY
6622101
NiCrAlY
70 2 6||tt| |NiCoCrAlY
46 23 17 13
NiCoCtAlY
47221713
NiCoCrA/YSiHf
47221713
CoCrAlY
632313| |tt||GB/T 19356--2003
0. 4 ~0. 60. 3 ~0. 5
0, 1~0, 5
Chemical composition/(%)
15-~1911.5~13.52026
15~191
11,5-~13, 20~24||tt| |22--24
11. 8--13, 2 20-- 24
0. 8~1. 2
0. 2 ~0. 7||tt| |0.2--0.6 0.4~-0.8
0.55--0.75
0.1-0.4
GB/T19356—2D03|| tt||Abbreviation code
CoNiCrAEY
38 32 21 8
CoCrNiAIYTa
52 25 10 7.5
FeCrAlY
74 20 5
Abbreviation code
NiAl 95 5
NiAI7030
NiA18020
NiAlMo 90 5 5
NiAIMo 89 10 1
FeNiA 51 38 10
FeNiAIMo 54 35 5 5
Abbreviation code
X42C-r13
X105C -Me17
X2CrNi 18 9
X5CrNi18 9
: 10--12.5
6. 5;X2CrNiMe 18.10
e. 8 X2CrNiMo 18 12
31--33
Table 5 (continued)
20--22
23~-27| |tt||Chemical composition/(%)
Ni-AI-Fe metal alloy material powder
Chemical composition/()
11.5~13.5
28- -32
18-~22
1 0. 5~1. 5
High alloy steel
0. 35 ~~0. 65
0. 3~0, 7
Chemical composition/(%)
Residue p,3~0. 5b. 2~0. 4
6. 4-- 0, 8
16. 5~18, 3 2--2. 5
36. $~18. 5/ 2. 5~3
6. 7 17 13
X2NiCrMoCu
25 20 5
X130CrMoWV
11, 5 -..
24 ~26
16.5~18.52.5~3.0
19~-21
[SO14332:2000
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