QB 1772-1993 Benzyl Propionate QB1772-1993 Standard download decompression password: www.bzxz.net

Industry Standard of the People's Republic of China
QB1769~-1801-93
Fragrance Standard
(Product Standard)bZxz.net
Published on April 29, 1993
Implementation on December 1, 1993
Published by the Ministry of Light Industry of the People's Republic of China
Subject Content and Scope of Application
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Industry Standard of the People's Republic of China
QB1772·93
Phenyl Propionate
This standard specifies the requirements, test methods and test contents of benzyl propionate. This standard applies to the internal acid station prepared by esterification of propionic acid and benzyl propionate. Reference standards
GB/T14454.3 Determination of color of spices
GB/T14454.2 Evaluation of aroma of spices
GB/T14454.4 Determination of refractive index of spices GB/T144540 Determination of relative density of isolated and synthetic spices GB/T14157.4 Determination of acid content of isolated and synthetic spices GB/T14457.5 Determination of fat content of isolated and synthetic spices GB/T14467.1 Determination of ester content of 3. Product chemical name, molecular formula, structural formula, molecular weight Chemical name Propionic acid
Molecular formula CH,O
Formula CH,CH,COOCH,H
Quantity 184,21 (according to the 1987 international atomic weight) 4 Technical requirements
4.1 Color Colorless bright filter, color does not catch up with the color standard No. 4. 4.2 Aroma Fruity aroma, with lyric aroma. 4.3 Relative density (25/25) 12~1.
4.4 Xinguang rush number (200) 1.4960~1.50094.5 Acid value ≤1.0.
46 Ester content () 9.0
4.7 Hydrolysis time (25) 1ml of sample is completely dissolved in 70% (V/V) ethanol mlt. ,5 Test methods
5.1 Color inspection
QGB/T14454.3
People's Republic of China Ministry of Light Industry 1993-04-28 approved 193121 bottle
—15-
5.2 Aroma evaluation
ECR/T14454.2..
5.3 Relative ratio determined at 23/25℃
5.4 Determination of refractive index, 2 sources
GB/T 14454.1.
5.5 Determination of alcohol content
GB/TJ4457.4
5.6 Determination of ester content
ACB/T 14157.5..
Note: Color
5.7 Determination of solubility, 25℃
See /T14457.1.
6 Inspection rules
Q51772-93
6.1 Each batch of finished products of propionic acid carbendazim shall be supervised by the production inspection department. The manufacturer shall ensure that all products leaving the factory meet the requirements of this standard. Each batch of products leaving the factory shall be accompanied by a quality certificate, which shall include: small name, product name, trademark, factory date, batch number, net weight, product quality certificate and standard abbreviation of this standard. 6.2 The acceptance unit has the right to confirm the various specifications of this standard and inspect whether the quality of the products received meets the requirements of this standard. The batch numbers of 2016-2017 are inspected and accepted for the first time, and different batch numbers are inspected and accepted separately. The packaging units of the 2016 batch are less than 1 box and the tax is collected in batches of 1 (bottle). When opening the package to take out the milk, check the appearance and see if there is any moisture or impurities. After heating, filter it evenly, then use a glass sampling tube (bottle) to absorb 0-1 μm of the sample, inject it into a mixer and mix it evenly, and put it into two small bottles standing by the cold detector. Note: "manufacturer name", "product name", "batch number", "date of collection", one bottle for inspection, and one bottle for confidentiality.
6.4·If one indicator in the acceptance invoice does not meet the requirements of this standard, the manufacturer may review and re-test it together with the manufacturer. If the annual inspection result still fails, the product batch will be re-accepted. 6.5 When the supplier and the manufacturer have disputes over the quality of the product, the two parties may jointly propose a solution and invite the inspection agency to assist. The cost shall be borne by either party.
6.6 Blood test, loss Gas, acid value, phenol content or other parameters are factory inspection indicators. Density, washing volume and solubility are type inspection indicators and are inspected once every year.
7 Marking, packaging, transportation and storage
7.1 The products are packed in galvanized barrels or glass barrels. The outside of the packaging is marked with: product name, manufacturer, trademark, batch number, net weight, export date, label number and related packaging marks. If there are special requirements for individual orders, they can be negotiated with the manufacturer. 7-2 The products should be kept away from rain and foreign air pollution during transportation. It is strictly forbidden to transport with acids, radiants, etc. 7.3 The products should be stored in a non-flammable, ventilated and cool warehouse to prevent foreign air pollution and stay away from fire sources. 7.4 The warranty period of this product is one year if the transportation conditions are met, the packaging is received and the product is unsealed. 5
A Instrument
Q8 177293
Appendix A
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Determination of Propylene Content by Gas Chromatography Internal Normalization Method (Closed Reference Document)
A1.1 The chromatograph, recorder and microprocessor are in accordance with the provisions of Article 5 of GB11539. The filling column is 2 to 3m long and has an inner diameter of 4m.
Determination of PFG ,5-1 Example JChromoaorh
WAWDMCS60--OEL.
A1.3 Detector
Oxygen initial ionization detector.
A2 Operation example
A2,1 Spectrometer furnace linear program external temperature from -0 it, rate 3/min or 160cti temperature.
Inlet 11210,
Light: 210.
A2.2 Flow rate
Carrier gas wash gas, 25ml/mi m
A3 Determination of efficacy
A5.1 Chemical properties test
The test shall be carried out in accordance with the provisions of Article 8.1 of GB11539 and shall meet the requirements.
A3.2 Effect
According to the method specified in Article 3 of GB11539, the properties of the product shall meet the requirements.
A4 Determination method
The internal chemical method shall be carried out in accordance with the method specified in Article 10.4 of GB11559. A5 Repeatability and result expression
According to the provisions of Article 11.1 of GB115394, the test shall meet the requirements. 17
Additional instructions,
081772-93
This standard is issued by the Quality Standards Department of the Ministry of Light Industry. This standard is under the jurisdiction of the National Materials Standardization Center of Shandong Province: This standard was drafted by the Xinxia Spice Factory of Shandong Province, and the main drafter of this standard is Luo Jian.
This name is based on the American Essential Oil Association standard E0A20.209. From the date of implementation of this standard, the Ministry of Light Industry standard QB906. Intrinsic Acid will be invalid. 18
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